IKA C 5000 control Package 2/12 User Manual

Page 74

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IKA

-WERKE C 5000 control/duo-control Ver. 10 04.07

3DJH 

d

Suspend carefully the decomposition vessel into the open measurement cell cover

until it reaches the stopper (1., see the following illustration).

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The decomposition vessel maintains a defined position in the holder on the fill head

by being lowered at the centre of the fill head by 0.8 mm (no. 2 in the following illus-

tration). A spring element then contacts the electrical ignition contact on the decom-

position vessel.

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The message "Bomb securely closed?" will appear. Ensure that the decomposition

vessel is properly closed and confirm with OK.

The message

%RPE

p

on the bottom line of the screen changes to a display of the

function key assignment

6WDUW

If the function key assignment

6WDUW

does not appear,

please check the ignition wire of the decomposition vessel. Take note of whether the

status is shown in a

6WDEOH

state on the display.

After each measurement, the measurement cell is adjusted so that normal starting

conditions are present for the next measurement. During this phase (about 3 to 5

minutes), “Unstable!!” is displayed in the process window of the measurement cell.

As long as this message is displayed, no measurements are possible in adiabatic or

isoperibolic operating modes. Experiments in dynamic mode can also be started

during the adjustment phase.

In addition to the adjustment requirements, the following conditions must be fulfilled

in order to start a measurement:

A measurement must be prepared

The maintenance function must not have been activated

The decomposition vessel must be removed and placed back in again

The ignition contact and the ignition wire of the decomposition vessel being

used must be in order.

Not until this point is the start button for the measurement cell enabled, i.e.,

6WDUW

appears on it.

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