2 control with «ic cap» (automated operation), Control with «ic cap» (automated operation) – Metrohm 761 SD Compact IC User Manual

Page 94

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5 Operation

761 SD Compact IC / Instructions for Use 8.

761.1043

86

5.2.2

Control with «IC Cap» (automated operation)

Start the «IC Cap» software and log in (see Section 2.12.4).

Configuration

auto.cfg

should have been installed during installation

(see Section 2.12.2). If not, now load configuration

auto.cfg

(see Sec-

tion 4.2.1).

With automated sample change, it is possible to predefine the se-

quence of conditioning, calibration and sample determination with a

sample table (queue).

5.2.2.1

Preparing sample vessels (automated operation / «IC Cap»)

1 Prepare calibration standards

Fill each of the 6 sample vessels with an MCAL standard

(150, 250, 350, 450, 550 and 650 mg/L H

3

PO

4

plus basic con-

tent of nitrate and sulfate) and position them at the required

position in the sample rack of the 766 IC Sample Processor.

The MCAL standard bottles are supplied as accessories

(6.2321.000).

2 Prepare the samples

Fill sample vessels with the samples to be measured and po-

sition them at the required position in the sample rack.

3 Prepare the rinsing solution

Fill the special beakers at the rinsing position of the 766 IC

Sample Processor with ultra-pure water.

5.2.2.2

Creating a sample table (automated operation / «IC Cap»)

After opening «IC Cap», the sample table (queue) should be dis-

played at the left-hand side of the screen (if configuration

auto.cfg

is

loaded).

Create the sample table (see Administrator Manual «IC Cap 2.0»,
Section 2.3
). First perform a conditioning step with system

startup.smt

. Then perform the calibration measurements and the

sample determinations with the system

auto.smt

. Assign the number

for

Vial

to the rack positions you have selected.

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