4 reagents, 1 reagent 1, 2 reagent 2 – Electro-Chemical Devices (ECD) CA6 Hardness Analyzer User Manual

Page 80: 1 reagent 1 11.4.2 reagent 2

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11.4 Reagents

!

For reagent preparation use demineralised water and analytical quality reagents.

DANGER:
Read the precaution and (MSDS) datasheets and wear protective gloves, clothes and glasses

before use of chemical products.

11.4.1 REAGENT 1
CA6 Hardness reagents

Reagent 1

Cresolphthalein Solution
Part Number# 2010037-1

For 1 Liter preparation:
Name

Quantity

Hydrochloric Acid 37%, ACS Reagent

CAS Number: 7647-01-0

2.83 ml/L

o-Cresolphthalein Complexone

CAS Number: 2411-89-4

0.075 g/l

Clean all equipment with DI water before use.

Dissolve o-cresolphthalein in 2.83 ml of the concentrated hydrochloric acid. It may take a minute or so.
Fill a 1 liter volumetric flask to 2/3rds capacity with DI water. When dissolved slowly add the
Cresolphthalein HCl solution to the water while stirring the solution. Fill the volumetric flask to the
gauge line (1 liter). Transfer to the reagent 1 container provided with the analyzer.

11.4.2 REAGENT 2

Reagent 2

Ethanolamine solution
Part Number# 2010038-1

For 1 Liter preparation:

Name

Quantity

Ethanolamine, ACS Reagent

CAS Number: 141-43-5

200 ml/L

Deionized Water

800 ml

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