Able, 10: epa z, Alibration – Teledyne 6200A - Sulfides analyzer User Manual

Page 121: Rocedure

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TAI Model 6200A SO

2

Analyzer Operator Manual, 02164, Rev. G

Zero calibration procedure.

Table 7-10: EPA Zero Calibration Procedure

Step Number

Action

Comment

1.

Press CAL

The 6200A enters the calibrate mode from sample mode.
Allow the zero gas through the sample port.

2.

Wait 10 min

Wait for reading to stabilize at the zero value.

3.

Press ZERO

To select a zero calibration.

4.

Press ENTR

Pressing ENTR actually changes the equations

5.

Press EXIT

6200A returns to the CAL menu.

1. Adjust the SO

2

concentration to approximately 80% of the URL of the range. The expected

SO

2

span concentration can be determined by measuring the cylinder and diluent flows and

computing the resulting concentration.

Calculate the expected concentration as follows.

[

]

[

]

SO

F

F

SO

gas

total

ga

2

=

×

s

----------------------------------- Equation 7.1

2

where;

[SO

2

]

gas

= cylinder gas concentration, ppm

F

gas

=

SO

2

gas flow rate, cc/min.

F

total

= total(gas + diluent) flow rate, cc/min.

[SO

2

]

= expected SO

2

concentration, ppm

Enter the expected concentration [SO

2

] using the procedure in Table 7-12. The expected span

concentration need not be re-entered each time a calibration is performed unless it is changed.

7-14

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