Application example – VACUUBRAND MV 10 NT VARIO User Manual

Page 58

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page 58 of 126

Attention: If the controller is set to ”Defaults”: On”, all stored pro-

grams will be deleted.

Example

NT VARIO vacuum pump with speed control (e.g., with a rotary evap-

orator): Degassing and automatic distillation with timing

Program step 1 should be always a definite initial state, here atmospheric

pressure (ATM). To reach this state definitely, set a tickmark at ”Vent.”

and ”Step” by pressing the selection knob.

In step 2, pumping begins, attempting to reach 300 Torr/mbar as quickly

as possible (”Step”). Vacuum holds there for 10 minutes (degassing the

solvent).

In step 3, ”Auto

” causes an automatic search of a boiling point in

the pressure interval between 300 Torr/mbar/hPa (depending on preset

pressure unit) and 2 Torr/mbar/hPa, followed by automatic adaptation to

changes in the boiling point. The following step starts either (1) once the

cumulative process time reaches the set limit (1 hour/60 minutes), even

if the preset pressure (2 Torr/mbar/hPa) has not been reached, or (2) if

a vacuum of 2 Torr/mbar/hPa is reached, even if the preset time has not

been completed.

Step 4 vents to atmospheric pressure as fast as possible and switches off

the control after one minute.

Program

No hh:mm:ss Vac Vent. Step Auto

01 00:00:00 ATM

✔ ✔

02 00:10:00 300

03 01:00:00 2

*

04 00:01:00 ATM

✔ ✔

05 00:00:00 0

06 00:00:00 0

07 00:00:00 0

08 00:00:00 0

09 00:00:00 0

10 00:00:00 0

- - - - - - - - - - - - - Back - - - - - - - - - - - - - -

01:11:00

* If the pressure difference

between the vacuum for

degassing and the expect-

ed vacuum for distillation is

very small (distillation vac-

uum >75% of the degas-

sing vacuum), select the

function ”Auto ” (adapting

the vacuum starting from

the current pressure) in-

stead of ” Auto

” (at first

searching the boiling point

automatically, and then

adapting the vacuum).

Application example

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