2 mode of operation, 1 principle of the rotational vacuum concentration – Martin Christ RVC 2-33 CDplus User Manual

Page 13

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Rotational Vacuum Concentrator RVC 2-33 IR

2 Layout and mode of operation

Version 08/2009, Rev. 2.1 of 02/12/2014 • sb

13

Translation of the original operating manual

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2.2 Mode of operation

Pos: 24 / 200 Christ /37 0 RVC-BA (STANDARDM ODULE)/ 020 Au fba u un d Wirku ngsw eise/0 20- 002 0-0 010 Prinzip de r Rot ations -Vaku um-K onze ntra tion @ 25 \mo d_1 404 9849 804 90_ 68.d ocx @ 186 631 @ 3 @ 1

2.2.1 Principle of the rotational vacuum concentration

This method is used for the particularly quick and gentle evaporation,
drying, purification, and concentration of samples.
Rotational vacuum concentration is an alternative to rotary evaporators that
use high temperatures and operate nearly at normal pressure. Because of
the vacuum, the sample boils at low temperatures, and water as well as
organic solvents can be evaporated in a particularly gentle manner. Due to
the fact that the sample rotates like in a centrifuge, the

Boiling retardation

is prevented so efficiently that low pressure can be used. As a result,
temperature-sensitive samples can be concentrated by evaporation without
being damaged.
The solvent can be collected in a cooling trap and disposed of immediately
if desired.

Fig. 3: Vapour pressure curve for ice and water

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