Procedure – LaMotte SMART Spectro Spectrophotometer User Manual

Page 87

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PROCEDURE

Use universal sample holder

1. Press and hold ON button until spectrophotometer turns on.
2. Scroll to and select PROGRAMMED TESTS.
3. Scroll to and select ALL TESTS (or another sequence containing

21 Chloride-TT) from TESTING MENU.

4. Scroll to and select 21 Chloride-TT from menu.
5. Rinse a tube (0290) with sample water. Fill to 10 mL with sample.
6. Insert the tube into chamber, close lid and select SCAN BLANK.
7. Remove the tube from Spectro.
8. Add one *Chloride Spectrophotometric Grade Tablet (3885A).
9. Use Tablet Crusher (0175) to crush tablet.
10. Cap tube.
11. Invert 2 times.
12. Wait 3 minutes. Do NOT mix.
13. Insert tube into chamber, close lid and select SCAN SAMPLE. Record result

in ppm chloride.

14. Press OFF button to turn the colorimeter off or press EXIT button to exit to a

previous menu or make another menu selection.

NOTE: For best possible results, a reagent blank should be determined to account

for any contribution to the test result by the reagent system. To determine the

reagent blank, follow the above test procedure to scan a distilled or deionized

water blank. Then follow the above procedure to perform the test on a distilled or

deionized water sample. This test result is the reagent blank. Subtract the reagent

blank from all subsequent test results of unknown samples.

The reagent system is temperature sensitive. The calibration is for 25ºC. If sample

is at 30ºC, multiply resulting ppm by 1.1. If the sample is at 20ºC, multiply resulting

ppm by 0.9.

CHLORIDE, TesTab

SMART Spectro Test Procedures 2.11

Test P

rocedures

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