3 attaching the accessories, Attaching the accessories, Capillaries – Metrohm 818 IC Pump User Manual

Page 15: Pulsation dampener, Fig. 3, Connect capillaries

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2.3 Attaching the accessories

818 IC Pump / 8.818.1023 Instructions for Use

9

2.3

Attaching the accessories

2.3.1 Capillaries

Some of the connections under high pressure between the 818 IC

Pump and the IC system must be set up by the user, see section 2.4.

For that the 6.1831.010 PEEK capillary (i.d. = 0.25 mm, o.d. =

1

/

16

"

,

length = 3 m) supplied in the accessories of the 818 IC Pump can be

used.

Capillaries fitted with new connectors must have a perfectly flat cut

surface. For PEEK capillaries it is best to use the

6.2621.080

Capillary tubing cutter

Fig. 3:

Connect capillaries

19 PEEK capillary (6.1831.010)


20 Compression fitting (6.2744.010)

For the connection of 6.1831.010 PEEK capillaries or of the 6.1834.000

PTFE aspirating tubing, the supplied 6.2744.010 PEEK Compression

fittings are used. It is best to proceed as follows:

1 Mount compression fitting

Slide a compression fitting 20 (6.2744.010) over the end of the

capillary 19 to be fastened as shown in Fig. 3.

2 Insert capillary in connection

Push capillary end in the corresponding connection as far as it

will go (to avoid dead volume).

3 Tighten compression fitting

Tighten compression fitting 20 by hand (never use tools).

2.3.2 Pulsation

dampener

To protect the column material against pressure drops caused by the

injector, the use of a pulsation dampener connected between the pump

and the injection valve of the 820 IC Separation Center is

recommended. The optional 6.2620.150 Pulsation dampener MF is

very well suited to this purpose (see section 6.3).
The metal-free 6.2620.150 Pulsation dampener is supplied fully

assembled and has two connections for capillaries, for which two

20

19

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