Viscometer tubes, Dual-solvent washing, Thermistor operation – Cannon Instrument miniAV-X User Manual

Page 82: Timing bulb determination

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CANNON

®

miniAV-X Automatic Viscometer with VISCPRO

®

Instruction & Operation Manual

Version 1.Ob— March, 2012;

CANNON

®

Instrument Company

2139 High Tech Road • State College, PA 16803 • USA

76

WARNING

Waste sample/solvents can present possible environmental and health
hazards. Dispose of all waste materials in accordance with environmental
and safety regulations.

Dual-solvent washing

For testing heavy or hard-to-clean materials,

CANNON

®

Instrument

Company recommends a dual-solvent washing system. The dual-solvent
washing process uses two different solvents. The first wash might
ordinarily use a heavy solvent to clean the sample residue out of the
viscometer tubes. The second wash might use a lighter solvent to remove
any remaining sample/solvent residue and dry the viscometer tube. Test
temperature(s) must be carefully considered when choosing solvents.

Dual-solvent action

To engage the dual-solvent washing, make certain that desired wash
options are selected in the VISCPRO

®

software for

Solvent A

(washing

solvent) and

Solvent B

(drying solvent). Follow the instructions in the

Installation section of this manual to correctly configure the instrument
for dual solvent operation.

Viscometer tubes

The miniAV-X is equipped with a borosilicate glass capillary viscometer
tube having a wide viscosity range. The upper viscosity limit is up to 100
times the lower viscosity limit, depending on the tube type. Each 100-
fold viscometer tube contains three thermistors used for sensing the level
of the sample within the tube.

Thermistor operation

The tube thermistor detects the change in thermistor temperature associ-
ated with the passing of the sample meniscus, and records the time
accurately to within one-hundredth (0.01) of a second.

Timing bulb determination

As the sample is drawn into the viscometer tube, the VISCPRO

®

software

automatically determines which timing bulb will be used to test the
sample.

The sample will be drawn into the bulb above the upper timing ther-
mistor. That bulb will serve as the overflow bulb for that particular test
run.

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1

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>

NOTE

The numbers listed in this table are approximations, not absolute values.

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