Metrohm 889 IC Sample Center User Manual

Page 6

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Table of contents

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IV

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889 IC Sample Center

4.3

Full loop injection ............................................................... 21

4.4

Partial loopfill injection ...................................................... 24

4.5

Pickup injection .................................................................. 27

5 Handling and maintenance

31

5.1

General ................................................................................ 31

5.2

Care ...................................................................................... 31

5.2.1

Cleaning in general ................................................................ 31

5.3

Maintenance and service ................................................... 32

5.3.1

Sample loop .......................................................................... 32

5.3.2

Replacing the sample needle ................................................. 33

5.3.3

Replacing the air needle ........................................................ 35

5.3.4

Replacing the fuses ................................................................ 36

5.4

Quality Management and validation with Metrohm ....... 37

6 Troubleshooting

38

6.1

Error list .............................................................................. 38

6.1.1

Rack unit ............................................................................... 38

6.1.2

Needle unit ............................................................................ 39

6.1.3

Syringe unit ........................................................................... 40

6.1.4

Injection valve unit ................................................................. 42

6.1.5

Cooling unit .......................................................................... 42

6.1.6

Electronics ............................................................................. 42

6.2

Analytical problems ............................................................ 43

6.2.1

Autosampler .......................................................................... 43

7 Appendix

45

7.1

Samples and sample vials .................................................. 45

7.2

I/O interface ........................................................................ 45

7.2.1

Properties of the I/O interface ................................................ 46

7.2.2

Pin assignment of the remote interface .................................. 46

8 Technical specifications

47

8.1

General ................................................................................ 47

8.2

Sampling .............................................................................. 47

8.3

Analytical characteristics ................................................... 48

8.4

Programming ...................................................................... 48

8.5

Interfaces ............................................................................. 48

8.6

Options (pre-installed) ........................................................ 48

8.7

Mains connection ............................................................... 49

8.8

Safety specifications ........................................................... 49

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