6 high-pressure pump, 1 removing the transport security screws, 2 installing the pulsation dampener (option) – Metrohm 790 Personal IC User Manual

Page 34: 6 high-pressure, Pump

Advertising
background image

2.6 High-pressure pump

790 Personal IC

25

2.6 High-pressure

pump

In order to avoid damage to the pump it must never be operated dry.

Each time that the pump is switched on always first check that the

eluent supply has been connected up correctly and that sufficient

eluent is present in the eluent bottle.


2.6.1

Removing the transport security screws

In order to prevent the pump drive from being damaged during trans-

port the pump head is fitted with three transport security screws 10

10

10

10 (see

Fig. 2). These transport security screws must be removed before the

high-pressure pump is started up. Also remove the red sticker attached

to the pump head 34

34

34

34.

In order to avoid damage to the pump head these three security

screws should be attached to the pump head each time that it is to

be transported.

2.6.2

Installing the pulsation dampener (option)

To protect the column material of sensitive separating columns (e.g.

methacrylate-based columns) against pressure drops caused by the in-

jector, the use of the optional

6.2620.150 Pulsation dampener MF is

recommended. It has to be installed between the high-pressure pump

and the injection valve of the 790 Personal IC as follows (see Fig. 10):

1 Install pulsation dampener

• Position the pulsation dampener 52

52

52

52 in the interior of the 790

Personal IC on the base.

2 Connection to the pump

• Unscrew PEEK capillary 27

27

27

27 of coupling 26

26

26

26 and attach it to

connection 54

54

54

54 of the pulsation dampener 52

52

52

52.

3 Connection to injection valve

• Unscrew PEEK capillary 18

18

18

18 of coupling 26

26

26

26 and attach it to

connection 53

53

53

53 of the pulsation dampener 52

52

52

52.

The pulsation dampener is filled with isopropanol and must be rinsed

with eluent before connection to a separating column (see section

2.6.4).

The 6.2620.150 Pulsation dampener can be operated in both direc-

tions.

Advertising