4 .2 measuring cells and their modes – BUCHI NIRFlex N-500 User Manual

Page 20

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4 Description of function

20

NIRFlex N-500 Operation Manual, Version F

Data processing and interferogram analysis
The NIR light interacts with the sample G material in different ways, leaving a characteristical finger-
print on the interferogram. At liquids the light is mostly transmitted and at solids reflected. The
remaining light is collected by the detector H. The built-in computer further processes the raw signal.

Process steps

Result

Signal preprocessing

Interferogram

Fourier transformation

Raw spectrum

Signal background correction

Spectrum of sample

Chemometric analysis of the spectral data

Sample analysis

Display of the result via NIRWare Operator on the attached monitor

Sample analysis is displayed

4 .2

Measuring cells and their modes

The NIRFlex N-500 system is of modular design. The interferometer is located in the basic instrument.
Different measuring cell modules for different kinds of sample materials can be easily attached to the
basic intrument. To choose the best measuring cell for a specific range of samples the optical proper-
ties of the sample material must be know.

Measuring cell matrix

Sample characteristics

(for NIR light)

Section

Measuring cell

Typical application

Diffuse reflection

4.2.1

NIRFlex Solids;
NIRFlex Fiber Optic Solids;
NIRFlex Fiber Optic SMA*

Predominantly non-translucent
materials such as most tablets,
cereals and powders

Transmission

4.2.3

NIRFlex Liquids;
NIRFlex Fiber Optic Liquids
NIRFlex Fiber Optic SMA*

Translucent and transparent liquids

Diffuse transmission 4.2.4

NIRFlex Solids Transmittance

Predominantly translucent solids
such as some tables, crystal
powders and other light conducting
materials

Transflectance

4.2.5

NIRFlex Fiber Optic Solids / NIRFlex
Solids with Transflectance Adapter;
NIRFlex Fiber Optic SMA*

Solids with weak diffuse reflection
and low transmission rate charac-
teristics

*Depending on the custom accessory
and measurement setup

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