8 method "dialysis – Metrohm 766 IC Sample Processor User Manual

Page 92

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4.6 Standard methods

766 IC Sample Processor

87

>final sequence
>changer settings
rack number 0
lift rate 1 12 mm/s
shift rate 20
>manual stop
CTL Rmt: **************
CTL RS232:
------------

−

—— Settings for changer functions ——

−

—— Reaction to manual stop ———

Settings in the «IC Metrodata» program

Definition of IC method (analysis time, start parameters for IC instru-

ments 732, 733 and 709, etc.), additional association of this method

with the following time program for the 732 IC Detector:

Method / Equipment / Setup / Program / Text:

0.0

Puls_766_set

Set remote line 3 at 732/1 to 1 (s. below)

0.1

Puls_766_reset

Set remote line 3 at 732/1 to 0 (s. below)

0.2

Flag

end

Program end

Method / Equipment / Setup / Program / Remote configuration:

Puls_766_set

= **1*****

Set remote line 3 at 732/1 to 1

Puls_766_reset

= **0*****

Set remote line 3 at 732/1 to 0

Method / Equipment:

Start with method

Procedure at program start

1. Start 766 IC Sample Processor with <START>.
2. Create new queue in the program «IC Metrodata» and start it.

4.6.8

Method "Dialysis"

Application

IC determinations with automatic sample dialysis.

Interconnection

see Fig. 13 and section 2.3.9 as well as 754 Instructions for Use

Program of 766 IC Sample Processor

766 IC Sample Proc. 11111 5.766.0010
parameters
method Dialysis
number of sample: rack
>start sequence
1 CTL:Rm: INIT
>sample sequence
1 SCN:Rm : Pump1 ?
2 MOVE 1 : sample
3 LIFT: 1 : work mm
4 CTL:Rm: PROG R/S 1
5 SCN:Rm : Ready1

−

Report header with serial number and program ver-
sion

−

Method name

−

Number of samples to be processed (entire sample
rack)

−

Initialize remote interface

−

Waiting until 709 IC Pump runs

−

Move needle to sample position

−

Place lift with needle to working position

−

Start time program at 732

−

Waiting until 732 IC Detector sends ready signal

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