Metrohm 761 Compact IC User Manual

Page 188

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5 Notes – Maintenance – Faults

761 Compact IC

178

To install a new piston seal 112 the special tool 117 is used.

First the new seal is inserted firmly in the recess of tool 117

by hand (see Fig. 20B). The seal spring must be located on

the outside.

The tool 117 together with the seal is then inserted in the

pump head 42 and the seal pressed into the pump head re-

cess with the aid of tool 116 (see Fig. 20C).

The seal surface in the pump head

42

must not be damaged (avoid

contact with tool)!

5 Cleaning/replacement of inlet valve

113

and outlet

valve

114

Contaminated or blocked valves are cleaned by rinsing with

dist. water, RBS solution or acetone. The rinsing effect can be

reinforced by brief treatment in an ultrasonic bath (max. 20 s;

if longer the sapphire sphere of the valve can be damaged).

If this does not have the desired effect, the valves can be

disassembled as shown in Fig. 21. The valve components are

pushed out with the aid of a syringe needle inserted through

the upper opening in the valve housing 118. The individual

components are rinsed with dist. water and/or acetone, and

the sapphire sphere cleaned with a paper towel. The valve is

then reassembled in accordance with Fig. 21. The compo-

nents of the inlet and outlet valves are identical, they are dis-

tinguished only by the positioning of the sapphire sleeve 121

and the ceramic holder 123 (see Fig. 21).

Valves that fail to function faultlessly after such cleaning must

be replaced.

In the reinstallation of the inlet valve 113 or the outlet valve

114 on no account must the two outwardly identical valves be

interchanged. To determine which valve is which, note that

the liquid flows through the pump head from the bottom up.

The flow direction of the valves can be checked simply by

blowing through the clean valve. Both valves are installed with

the black face in the direction of the pump head (see Fig. 19).

If by mistake an inlet valve

113

is installed instead of the outlet valve

114

, an extreme pressure buildup occurs within the working cylinder,

which is not detected by the pressure transducer and will destroy the

piston seal

112

!

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