Ammonium – YSI 600DW-B Sonde User Manual

Page 77

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Sondes

Section

2


Select the

1-point option only if you are adjusting a previous calibration. If a 2-point or 3-point calibration

has been performed previously, you can adjust the calibration by carrying out a one point calibration.
Immerse the sonde in a buffer of known pH value and press

Enter. You will be prompted to type in the pH

value of the solution. Press

Enter again, and the screen will display real-time readings that will allow you

to determine when the pH and temperature readings have stabilized. Pressing

Enter will confirm the

calibration. Then, as instructed, press

Enter again to return to the Calibrate menu. This calibration

procedure adjusts only the pH offset and leaves the previously determined slope unaltered.

Select the

2-point option to calibrate the pH probe using only two calibration standards. In this procedure,

the pH sensor is calibrated using a pH 7 buffer and pH 4 buffer. A two point calibration procedure (as
opposed to a 3-point procedure) can save time if the pH of the media being monitored is known to be either
basic or acidic. For example, if the pH of a pond is known to vary between 5.5 and 7, a two-point
calibration with pH 7 and pH 4 buffers is appropriate. Three point calibration with an additional pH 10
buffer will not increase the accuracy of this measurement since the pH is not within this higher range.

To begin the calibration, immerse the sonde in one of the buffers and enter the actual pH value. Press
Enter, and the screen will display real-time readings that will allow you to determine when the pH sensor
has stabilized. Pressing

Enter will confirm the calibration. Following the instructions on the screen, place

the sonde in the second pH buffer, input the pH value, press

Enter, and view the stabilization of the values

on the screen in real time. After the readings have stabilized, press

Enter to confirm the calibration. Then,

as instructed, press

Enter again to return to the Calibrate menu.


Select the

3-point option to calibrate the pH probe using three calibration solutions. In this procedure, the

pH sensor is calibrated with a pH 7 buffer and two additional buffers. The 3-point calibration method
assures maximum accuracy when the pH of the media to be monitored cannot be anticipated. The
procedure for this calibration is the same as for a 2-point calibration, but the software will prompt you to
select a third pH buffer to complete the 3-point procedure.

ORP

Select

5-ISE2 ORP to calibrate the ORP sensor. Immerse the sonde in a solution with a known oxidation

reduction potential value (we recommend Zobell solution) and press

Enter. You will be prompted to enter

the ORP value of the solution. Press

Enter, and monitor the stabilization of the ORP and temperature

readings. After no changes occur for approximately 30 seconds, press

Enter to confirm the calibration.

Then, as instructed, press

Enter again to return to the Calibrate menu.


The following calibrations are for the 6920DW sonde only. If you do not have this sonde, skip to
Section 2.9.6, Report.

AMMONIUM

When selecting

6–ISE3-NH4+, you will be given the choice of 1-point, 2-point, or 3-point calibrations for

your ammonium (NH

4

+

) sensor.


Select the

1-point option only if you are adjusting a previous calibration. If a 2-point or 3-point calibration

has been performed previously, you can adjust the calibration by doing a one point calibration. Immerse
the sonde in any solution of known ammonium concentration and press

Enter. You will be prompted to

type in the NH

4

+

value (in mg/L of NH

4

-N) of the solution you are using. Press

Enter again, and the screen

will display real-time readings that will allow you to determine when the NH4

+

readings have stabilized.

Pressing

Enter will confirm the calibration.


Select the

2-point option to calibrate the NH

4

+

probe using only two calibration standards that are both at

approximately the temperature of your environmental sample. In this procedure, the NH

4

+

sensor is usually

YSI Incorporated

Drinking Water Monitoring Systems Operations Manual

2-70

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