Cooling profile limitations, Profile designer test parameters – Cannon Instrument CMRV-5000 User Manual

Page 90

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84

CANNON

®

Mini-Rotary Viscometer

CMRV-5000 Instruction & Operation Manual

Version 1.0b—August, 2011; CANNON

®

Instrument Company

2139 High Tech Road • State College, PA • 16803 • USA

TO delete the point click Yes. To keep the selected point(s) click No.

Cooling profile limitations

CMRV cooling capacity

The CMRV cooling capacity changes proportionally with the tempera-
ture at which the instrument is controlling. Greater cooling capacity is
achieved at warmer temperatures, and capacity decreases as temperature
decreases. This makes linear rates-of-cooling impossible in relatively
short time frames.

Correcting profiles

If the rate-of-cooling for a profile exceeds the cooling capacity of the
instrument, one of three things must be done:

 Lengthen the time between the two fixed temperature points
 Decrease the temperature change between the two fixed times
 Apply a combination of the two previous options.

When a profile data point with a specified tolerance is entered in the
Profile Designer, software calculations are automatically made to deter-
mine if the rate-of-cooling relative to the previously-entered point is
within the instrument’s capability. It is assumed that the instrument can
achieve the temperature specified by the previous point. If no tolerance is
specified for that point, then this assumption may or may not be war-
ranted. For this reason, it is possible to design a profile that the instru-
ment is incapable of achieving. The software will only flag those points
that are absolutely impossible to realize. This suggests that experience
and experimentation are needed to properly design profiles which can be
run successfully.

NOTE

The ASTM D 3829 and ASTM D 4684 profiles supplied with the MRVW
software define non-toleranced points which are outside of the
instrument’s capability, but these are merely necessary stepping stones
which permit the instrument to attain proper temperature control at the
subsequent temperatures that are toleranced.

Profile Designer test parameters

The Profile Designer displays important test parameters for Yield Stress
and Viscosity testing. These values are editable from the Profile Editor.
For all ASTM profiles in the profile library, these values have been
preset in conformity with current ASTM specifications.

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