Metrohm 838 Advanced Sample Processor Manual User Manual

Page 74

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3.1 Sample racks

66

Metrohm 838 Advanced Sample Processor, Appendix

Special beaker positions

16 reserved rack positions with individ-

ual working heights, beaker radius and

beaker sensor test

The rack name is used for the unambiguous identification of a rack.

The standard name stored for the rack is the ordering number. In a

method, this can be assigned to a particular rack name (see Sec-

tion 2.3.1). The automatic rack recognition ensures that if an incorrect

rack is used this will be recognized and the user will be informed of this.
The code is used for automatic rack recognition. You must make sure

that this 6-place binary code coincides with the actual magnet code set

on the rack. Rack codes can be altered as required. However, they

must always be assigned to a single rack only. Avoid the use of the

predefined codes for the standard racks supplied by Metrohm, see also

p. 64.
The working position is used for defining the lift position at which a

sample is to be processed. This means that the ideal setting for a par-

ticular sample rack can be defined depending on the height of the

sample beakers. In manual operation this working position can be

moved to directly with the <END> key. In a run sequence this can be

programmed with

LIFT :1 : work mm

.

The rinsing position is used for defining the lift position at which, for

example, the electrode is to be rinsed. This means that the ideal setting

for a particular sample rack can be defined depending on the height of

the sample beakers. In a run sequence this can be programmed with

LIFT: 1: rinse mm

.

The shifting position is used for defining the lift position at which the

rack can be rotated. If the lift is located below the shift position then it

will be moved automatically to the shifting height before the rack is ro-

tated. This safety feature prevents the electrode from being damaged

by rotational movements of the rack to a large extent. However, a pre-

requirement is that this shifting height is set correctly. In a run sequence

the movement of the lift to the shift position can be programmed with

LIFT: 1 : shift mm

.

The special position is a further user-defined lift position. For example,

when pipetting with a robotic arm it can be selected so that the pipet tip

is located directly above the sample solution so that a separating bub-

ble (air gap) is formed. In a run sequence this can be programmed with

LIFT: 1 : special mm

.

The beaker radius can be used to prevent a titration head from trying

to enter a beaker which is too narrow for it, which could damage the

electrode or sample beaker. By entering the beaker radius a Sample

Processor can decide whether a titration or transfer head on the lift will

“fit” into the particular sample beaker, see also Section 2.2.
A beaker sensor is not available for the 838 Advanced Sample Proc-

essor at this time.

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