LaMotte SMART Spectro Spectrophotometer User Manual

Page 97

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PROCEDURE

Use universal sample holder

1.

Press and hold

ON button until spectrophotometer turns on.

2.

Scroll to and select PROGRAMMED TESTS.

3.

Scroll to and select ALL TESTS (or another sequence containing
23 Chromium-TT

) from TESTING MENU.

4.

Scroll to and select 23 Chromium-TT from menu.

5.

Rinse a tube (0290) with sample water. Fill to 10 mL with sample.

6.

Insert the tube into chamber, close lid and select SCAN BLANK.

7.

Remove the tube from Spectro.

8.

Add one *Chromium Spectrophotometric Grade Tablet (3889).

9.

Use Tablet Crusher (0175) to crush tablet.

10.

Cap tube.

11.

Shake vigorously for 30 seconds.

12.

Wait 3 minutes.

13.

Insert tube into chamber, close lid and select SCAN SAMPLE. Record
result in ppm chromium.

14.

Press

OFF button to turn the spectrophotometer off or press EXIT button

to exit to a previous menu or make another menu selection.

þNOTES: For best possible results, a reagent blank should be determined to

account for any contribution to the test result by the reagent system. To
determine the reagent blank, follow the above test procedure to scan a
distilled or deionized water blank. Then follow the above procedure to
perform the test on a distilled or deionized water sample. This test result is
the reagent blank. Subtract the reagent blank from all subsequent test results
of unknown samples.

To convert results to ppm chromate (CrO

4-2

), multiply by 2.23. To convert

result to ppm sodium chromate (Na

2

CrO

4

) multiply by 3.12.

Chromium-TesTab 1/2

SMART SPECTRO TEST PROCEDURES 04.08

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