6 appendix – Metrohm 817 Bioscan User Manual

Page 84

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6 Appendix

817 Bioscan

76

G

General information

on maintenance...............................58

General precautionary rules .................. 9
GLP ......................................................64

H

Handling of solvents .............................. 9
Handling the 817 Bioscan ...................35
Hazard ................................................... 8
Housing................................................68
Hydrodynamic voltammogram.......51,53

I

IC column

25

Figure................................................. 6

IC Net 2.1 .............................................36

817 Bioscan icon .............................36
817 Bioscan window .......................37
Configuration of MIC-9 ....................27

DC mode

..........................................39

Links

.................................................46

Manual

..............................................37

Manual control .................................33

Method parameters

..........................39

Program

............................................45

Program instructions .......................46

Pulse mode

......................................41

Scan mode

.......................................43

Scan mode - Operations

...................44

Scan mode - Parameters

..................43

Settings for MIC-8............................21
Time program for 766 / 788........23,31
Time program for 813......................23

IC Net 2.1 Icons

817 Bioscan .....................................36

IC Separating column

25

Mounting..........................................16

Immunity ..............................................68
Information about the

Instructions for Use............................ 7

Injection valve

Connection ......................................16

Injection Valve A

Connections.....................................26

Injection Valve B

Connections.....................................26

Installation............................................11
Instructions for Use 8.817.1003 ............ 7
Instrument description........................... 1
Instrument test with the dummy cell....63
Interference ..........................................50
Interior .................................................... 5
Introduction............................................ 1
Ion chromatography ............................55

K

KELF pressure screw (6.2744.130).....17

L

Leaks.................................................9,61
Links.....................................................46
Location ...............................................12

M

Mains cable

Connection.......................................14

Mains connection.................................14

Safety notes .......................................9
Technical data..................................66

Mains connection plug

17

Figure ............................................4,13

Mains switch

18

Figure ............................................4,13
On/off switching of the
instruments ......................................14

Mains voltage

Setting ..............................................12

Maintenance ...................................55,58
Malfunctions.........................................61
Manual control .....................................33
Manual valve

9

Figure .................................................4

Measuring cell......................see Flowcell
Measuring cell holder

22

Figure .................................................6

Measuring conditions ..........................48
measuring cycle...................................50
Measuring frequency ...........................50
Measuring interval................................50
Measuring potential ........................50,53

Optimization .....................................51

Measuring time ts ................................49
Method ...................................... 21,29,30

Method data

.......................... 39,41,43,45

Metrohm-Service..................................58
MIC-8

IC Net 2.1 - system configuration ....21
Installation ........................................20
Overview ..........................................11

MIC-9

IC Net 2.1 - System configuration ...27
Installation ........................................24
Overview ..........................................11

Microfiltration............................. 55,56,57

Mode

.....................................................37

Model plate

10

Figure .................................................4

Modular IC system

Installation ........................................11

Monograph

"Ion chromatography" ........................7
"Practical Ion Chromatography".........7

Mounting screw

4

Figure .................................................4

Mounting screws

36 of flow cell

Figure ...............................................17

Mounting the column ...........................16

N

Notation..................................................8
Notes....................................................55

O

Offset

......................................... 40,42,44

On/off switching of the instruments.....14
Operating mode..............................33,65
Operation .............................................35
Operation using «IC Net 2.1» ...............36
Optimization of the

measuring potential .........................51

Optimization of the PAD parameters .. 49
Outlet

13 for spilled liquid

Figure ................................................ 4
Precautionary rules ........................... 9

Oven

................................. 38,39,41,43,66

Oven

32

Figure ................................................ 6

Oven heating fan

33

Figure ................................................ 6

Oxide formation................................... 50

P

Packaging ........................................... 11
PAD - Pulsed amperometric

detection.......................................... 49

PAD parameters

Optimization .................................... 49

Parameters for the pulse mode .......... 34
Parts

Standard equipment ....................... 69

Parts and controls ................................. 2
Peak broadening ................................. 62
pH .............................................. 35,48,57
Pictograms ............................................ 8
Polishing disk (6.2802.100)................. 59
Polishing the working electrode.......... 59
Potentials ............................................. 49
Power consumption ............................ 66
Practical notes..................................... 55
Precautionary rules................................ 9
Precipitates..................................... 56,57
Preheating capillary

31

Figure ................................................ 6
Mounting ......................................... 16

Preparing the 817 Bioscan.................. 32
Pressure drop...................................... 62
Pressure rise........................................ 62
Pressure screw (6.2744.130)

Mounting ......................................... 16

Program instructions ........................... 46
Protection class................................... 14
Protective earth ................................... 14
Pulsation.............................................. 35
Pulsation absorber

30

Connection ...................................... 15
Figure ................................................ 6
Practical Notes ................................ 56

Pulsation Absorber (6.2620.150) ........ 35
Pulsations ............................................ 61
Pulse.................................................... 37
pulse frequency................................... 50
Pulse mode ......................................... 47

Parameters ...................................... 34

Pulsed amperometric detection

(PAD) ............................................... 49

Pump ........................... see 709 IC Pump

R

Range ........................................ 39,41,43
Reaction products............................... 49
Reactions............................................. 48
Rear ....................................................... 4
Rear panel

5/6

Figure ................................................ 5

Rectification of malfunctions............... 61
Recycling........................................ 57,58

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