Putting into operation without post column reactor, Putting into operation, 10 putting into operation – Metrohm 844 UV/VIS Compact IC User Manual

Page 62

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pressure screw (6.2620.000) 69.

2 Connect flow-through cell outlet

with 2.844.0010, 2.844.0030, 2.844.0110 and 2.844.0130:

• Cut a piece of 6.1831.010 PEEK capillary to the required

length and attach one end of it to outlet "OUT"

130 of flow-

through cell

42 using a compression fitting 64 (6.2744.010),

and place the other end in a waste container.

with 2.844.0020 and 2.844.0120:

• Attach a 6.1831.100 PEEK capillary (100 cm) to the outlet

"OUT" 130 of flow-through cell 42/ 62 using a compression

fitting 64 (6.2744.010), and place the other end in a waste

container.

with 2.844.0030 and 2.844.0130:

• Attach a 6.1831.100 PEEK capillary (100 cm) to the outlet

"OUT" 130 of flow-through cell 42/

62 using a compression fitting 64 (6.2744.010), and place the

other end in a waste container.

2.10 Putting

into

operation

2.10.1 Putting into operation without post column reactor

Before you start injecting sample solutions with Versions 2.844.0010 /
2.844.0030 / 2.844.0110 / 2.844.0130 (without post column reactor)

the whole system must be checked for leaks and conditioned with
eluent until a stable baseline has been achieved. Proceed as follows:

When inserting the column always make sure that it is inserted

correctly in the flow direction shown on the sticker (the arrow must

point in the flow direction).

1 Open and connect system

• Start the «IC Net» PC program, if it has not already been

started.

• Select

File / Open / System

in the main window. Open the

system file created in Section 2.5.4 for the 844 UV/VIS

Compact IC.

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