3 spectrum window, Spectrum window – Metrohm 844 UV/VIS Compact IC User Manual

Page 86

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Table of contents

T int, ms

Integration

time.

Entry range:

10

...

254 ms

T out, s

Measuring time per data point.

Entry range:

0.05

...

2.00 s

Data rate

Effective measuring time per data point. The

Data rate

is the particular whole number multiple

of the value

T int

that is closest to the value

T

out

.

The measurement of a data point is explained by using an

example:
Set values:

T int

= 15 ms,

T out

= 0.1 s

The calculated

Data rate

is 105 ms (the particular multiple of

T

int

that is closest to the value

T out

; in our example 7 times 15

ms). This means that the integration will be carried out 7 times

(each time for 15 ms) and then averaged to give a data point.

<Optimize>

Optimizes

T int

and adjusts the VIS lamp.

It should be done

• after exchanging a lamp (UV or VIS)
• if parts of the intensity spectrum are in the

overload ( > 60'000 , peaks cut)

• if the maximum of the intensity spectrum

of dist. water is too low (below 33'000)

Before clicking

<Optimize>

, the flow-through

cell should be rinsed and filled with dist.

water. There must be no air bubbles in the

flow-trough cell when clicking

<Optimize>

.

Operating hours

Operating hours of the lamps.

UV lamp, h

Display of the operating hours of the
UV lamp.

<Reset UV lamp>

Set operating hours of the UV lamp
to 0. Click it after replacing the UV
lamp.

VIS lamp, h

Display of the operating hours of the
VIS lamp.

<Reset VIS lamp>

Set operating hours of the VIS
lamp
to 0. Click it after replacing the

VIS lamp.

3.3.3 Spectrum

window

The

SPECTRUM WINDOW

can be opened with a right-hand mouse-

click on the 844 icon and then selecting the menu item

Spectrum

window

, or via the

button on the subtab

Manual/Detector

.

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