3 spectrum window, Spectrum window – Metrohm 844 UV/VIS Compact IC User Manual
Page 86
Table of contents
T int, ms
Integration
time.
Entry range:
10
...
254 ms
T out, s
Measuring time per data point.
Entry range:
0.05
...
2.00 s
Data rate
Effective measuring time per data point. The
Data rate
is the particular whole number multiple
of the value
T int
that is closest to the value
T
out
.
The measurement of a data point is explained by using an
example:
Set values:
T int
= 15 ms,
T out
= 0.1 s
The calculated
Data rate
is 105 ms (the particular multiple of
T
int
that is closest to the value
T out
; in our example 7 times 15
ms). This means that the integration will be carried out 7 times
(each time for 15 ms) and then averaged to give a data point.
<Optimize>
Optimizes
T int
and adjusts the VIS lamp.
It should be done
• after exchanging a lamp (UV or VIS)
• if parts of the intensity spectrum are in the
overload ( > 60'000 , peaks cut)
• if the maximum of the intensity spectrum
of dist. water is too low (below 33'000)
Before clicking
<Optimize>
, the flow-through
cell should be rinsed and filled with dist.
water. There must be no air bubbles in the
flow-trough cell when clicking
<Optimize>
.
Operating hours
Operating hours of the lamps.
UV lamp, h
Display of the operating hours of the
UV lamp.
<Reset UV lamp>
Set operating hours of the UV lamp
to 0. Click it after replacing the UV
lamp.
VIS lamp, h
Display of the operating hours of the
VIS lamp.
<Reset VIS lamp>
Set operating hours of the VIS
lamp to 0. Click it after replacing the
VIS lamp.
3.3.3 Spectrum
window
The
SPECTRUM WINDOW
can be opened with a right-hand mouse-
click on the 844 icon and then selecting the menu item
Spectrum
window
, or via the
button on the subtab
Manual/Detector
.