4 drift – Metrohm 787 KF Titrino User Manual

Page 20

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2.3. Tutorial

787 KF Titrino

16

It is now necessary to match the factor to the new result unit. A table with a selection of

matched quantities for factor, divisor and unit of the sample size can be found in the

quick reference.

<CALC DATA>

4 × <ENTER>

<1>

<ENTER>

<ENTER>

2 × <QUIT>

• Enter a new factor: Press <CALC DATA> and enter

the inquiries of the "calculation" group with

<ENTER>. Proceed with 3 times <ENTER> to the

display:

• Enter "1".

• As divisor enter the density of the sample.

• Exit the inquiry by pressing <QUIT> twice. The re-

sult is recalculated and outputted.

2.3.4 Drift

The drift is measured in µL/min. It specifies how much KF reagent is consumed per unit

time to keep the titration cell dry. The reagent is needed,


• to titrate moisture in the titration cell.
• to compensate the iodine consumption of slow side reactions.

The drift value is generally of the order of a few µL/min for "dry conditioned" titration cells.

Checking the condition of the solvent

The drift can be displayed during the conditioning of the titration cell with the <DRIFT>

key:

<DRIFT>

<DRIFT>

• Press <DRIFT>. The first line of the display shows

You can follow the progress of the drift. In fresh solvent

the drift value should drop to less than 10 µL/min after

a few minutes.


• Pressing <DRIFT> once again switches the drift

display off.

KFT volume

3.459 ml

factor 0.1

KFT volume

3.459 ml

divisor 1

Drift 4.3

µl/min

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