YSI 9300 Photometer User Manual

Page 111

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Test Procedure

1

Filter sample if necessary to obtain a clear solution.

2

Fill test tube with sample to the 10 ml mark.

3

Add one Molybdate No 1 LR tablet, crush and mix to dissolve.

4

Add one Molybdate No 2 LR tablet, crush and mix to dissolve.

5

Stand for two minutes to allow full color development.

6

Select Phot 42 on the photometer.

7

Take Photometer reading in the usual manner (see photometer instructions).

8

The result is displayed as mg/l MoO

4

.


Note
Molybdate concentrations can be expressed in a number of different ways. The

following factors may be used for the conversion of results :-

To convert from MoO

4

to Na

2

MoO

4

- multiply by 1.3

To convert from MoO

4

to Mo - multiply by 0.6.


Interferences

1

Copper 20 mg/l, zinc 20 mg/l, phosphate 100 mg/l and calcium 200 mg/l do

not interfere in this test.

2

Iron 10 mg/l and chlorine 10 mg/l cause slightly high blank readings equivalent to

0.6 mg/l Mo. However, they do not cause any interference in samples which
contain molybdate.

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