2 development of a method, titration of an acid – Metrohm 719 S Titrino User Manual

Page 15

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2.4

Tutorial

719 S Titrino

11

2.4.2 Development of a method, titration of an acid

Selection of the mode

<MODE>

<ENTER>

4 × <SELECT>

• Press <MODE> repeatedly until "SET" appears in

the display. For a description of the SET mode see

page 30ff.

• Confirm "SET" with <ENTER>

• Now select the measured quantity: Press

<SELECT> repeatedly until "pH" appears again in

the display.

Confirm the measured quantity "pH" with

<ENTER>.

Now set the end point.

Entry of the end point and the control parameters

<PARAM>

<ENTER>

<ENTER>

<ENTER>

<ENTER>

• Press <PARAM>. The display shows:

Control parameters for EP1


• Set the end point to pH = 7.00.

• Dynamics means the control range in which the

adding of the titrant is controlled in dependence on

the measured value (OFF: largest control range, i.e.

slow titration).

Set the range to 3. I.e. 3 pH units before the set EP

controlled dosing starts.

Maximum possible titration rate inside the control

range.

mode

mode SET

SET pH

********

SET: pH

SET pH

********

parameters

>SET1

>SET1

EP at pH

OFF

>SET1

EP at pH

7.00

>SET1

dynamics OFF

>SET1

dynamics 3

>SET1

max.rate 10.0

ml/min

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