Metrohm 763 PVC Thermomat Manual - Manual (Page 58)

4.4 Calibration functions
763 PVC Thermomat
51
11 Reaction vessel (6.1429.040)
22 Reaction vessel cover (6.2753.100)
66 Connecting tubing (6.1805.080)
for gas supply to reaction vessel
30 30 Connection nipple (6.1808.090)
31 31 Connection
Feedthrough for temperature sensor 36 36
33 33 Sealing ring (6.1454.040)
34 34 Connection
for connection nipple 30 30
35 35 Gas inlet tube (6.2418.000)
length = 148 mm
36 36 Temperature sensor Pt100 (6.1111.010)
37 37 Distance piece (6.2042.040)
Fig. 5: Accessories for Delta T determination
• Click on to open the Method parameters window. Enter the
required set temperature for the sample under Temperature
and set
Delta T
to
0°C
. Set
Gas flow
to the desired value and
click on <Save> .
5 Start gas flow and heating
• Switch on gas flow manually.
• Start heating for the selected block manually.
66
30 30
31
31
35
35
33
33
34
34
22
37 37
11
36 36
37 37