8 replacing the suppressor, Replacing the suppressor, Section 6.2.8 ) – Metrohm 761 SD Compact IC User Manual

Page 110

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6 Notes – Maintenance – Faults

761 SD Compact IC / Instructions for Use 8.

761.1043

102

6.2.8

Replacing the suppressor

The suppressor in the suppressor block may have to be replaced in the

following cases:

Irremediable loss of suppressor capacity (reduced

phosphate sensitivity and/or major rise in baseline)

Irremediable blockage of the suppressor

(Solutions can no longer be pumped through the sup-

pressor)

Both the suppressor rotor 6.2832.000 and the connector 6.2832.010

with the inlet and outlet capillaries can be replaced. Proceed as follows

in order to replace these components (see Figure 18):

1 Disconnect the suppressor from the IC system

Disconnect all inlet and outlet capillaries of the suppressor

from the IC system and peristaltic pump.

2 Dismantle the suppressor

Unscrew the nut 89 from the suppressor holder 92.

Pull out the connector 90 and suppressor rotor 91 from the

suppressor holder 92 (the connector and the rotor normally

stick together).

Detach the connector 90 from the suppressor rotor 91.

3 Clean the suppressor rotor

Clean the sealing surface of the new suppressor rotors 91

(6.2832.000) using a lint-free cloth and ethanol.

4 Insert the suppressor rotor

Insert the new suppressor rotor 91 in the suppressor holder

92 in such a way that the tubing connections at the rear of the

rotor fit in the corresponding openings inside the holder and

that one of the three holes in the rotor can be seen below in

the opening in the holder.

If the rotor has been inserted correctly, its sealing surface will

be approx. 4 mm inside of the holder. If this is not the case,

move the rotor into the correct position from below with the

aid of a sharp object (e.g. screwdriver).

5 Clean the connector

Clean the sealing surface of the new connector 90

(6.2832.010) with the aid of a lint-free cloth and ethanol.

6 Insert the connector

Fit the new connector 90 onto the suppressor holder 92 in

such a way that connection "1" is at the top and that the three

lugs on the connector fit in the corresponding openings of the

holder.

Screw the nut 89 onto the thread of the suppressor holder 92

by hand (do not use tools).

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