1 standard addition, Stan, Section 8.3.1 s – YSI TruLab 1320P User Manual

Page 54: Tandard, Addition

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Ion concentration

TruLab pH/ISE 1320

54

ba76157e01

03/2014

8.3.1 Standard addition

In the "Standard addition" procedure, a known amount of standard solution is
added to the sample.
The ion concentration in the sample is calculated from the change in potential.

Measuring

1.

Select the measuring method (see section 8.3 S

ELECTING

THE

MEASUR

-

ING

METHOD

, page 53).

2.

Prepare two standard calibration solutions.

3.

Perform a two-point calibration according to user guidance.

4.

The calibration record is displayed as soon as a stable value is
achieved for the second standard calibration solution.

CALIBRATION
12.12.2012 12:12:12
#1 0.010 mg/l

20.2 mV 25.0 °C

#2 0.100 mg/l

79.2 mV 25.0 °C

Slp.: 59.0 mV
Sensor +++ (Ion type: Ag)

12.12.2012

12:12

Continue

USB output

5.

Start the measurement with <F1>/[Continue].

An entry window appears.

6.

Prepare the sample.

7.

If necessary, add the ISA/TISAB solution to the sample.

8.

Thoroughly rinse the electrode with deionized water.

9.

Immerse the electrode in the sample.

10.

Using <> <> and <MENU/ENTER>, select the values for the vol-
ume of the sample (Sample volume) and the volume of the ISA/TISAB
solution (ISA/TISAB vol.).

i

Immerse sensor in sample

Sample volume

100.0 ml

ISA/TISAB vol.

1.0 ml

Continue

Standard addition

12.12.2012

12:12

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