Commissioning the vacuum – BINDER VD 23 User Manual

Page 74

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VDL (E2.1) 04/2014

page 74/107

13. Reference measurements. Checking the temperature in the inner

chamber

The controller display was adjusted in the factory to the temperature in the center of the usable volume

(chap. 19.1). The sensor probe of the reference measuring device was connected firmly to an expansion

rack positioned in the middle of the unit.
Checking the controller display

Conduct the reference sensor into the inner chamber through the measuring port (15). The port must

be largely vacuum tight to enable a typical operation vacuum for the calibration. For a high vacuum,

use a measuring access port (option). At low vacuum, a silicone plug with a hole for the sensor wire is

sufficient.

Fix the sensor to the center of an expansion rack in the middle of the useable volume with adhesive

aluminum tape or thermal conductive paste to ensure sufficient thermal conductivity.

Perform the measurement in a thermally stable condition with 3 expansion racks and empty oven.

Equilibrating time: at least 12 hours.

Checking the spatial temperature exactitude

Fix at least 9 sensor probes on 3 racks with adhesive aluminum tape or thermal conductive paste to

ensure sufficient thermal conductivity

The distance of the sensor probes to all inner chamber walls must be at least 10% of the correspond-

ing inner chamber dimension (see DIN 12880).

Perform the measurement in a thermally stable condition with 3 expansion racks and empty oven.

Response time: at least 12 hours.

Do NOT use the temperature probe of the reference measurement device without any contact

to the expansion rack, i.e., do NOT measure vacuum values!

In case the temperature probe is a thermo element, mount it so it is electrically insulated from

the rack.

If you note an excessive divergence between the controller and reference temperatures, please contact

BINDER Service to calibrate the temperature controller.

14. Commissioning the vacuum

With regard to operation, please observe the guideline BGI/GUV-I 850-0 on safe working in laboratories

(formerly BGR/GUV-R 120 or ZH 1/119 laboratory guidelines issued by the employers’ liability insurance

association) (for Germany).
Starting situation: The vacuum source is connected and ready for operation.
For the vacuum module with chemical membrane pump option, see chap. 15.3.

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