Metrohm NIRS XDS MasterLab Analyzer User Manual

Page 29

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27

Large Sample Cell, Reflectance

Detector Selection: Reflectance

Wavelength Range: 400-2500 nm

Preferred Spot Size: 17.25 mm

Aperture: Removed

Iris Adapter: Removed

This cell is optional, for large samples.

Vial Sampling in Iris Adapter, Reflectance

Detector Selection: Reflectance

Wavelength Range: 400-2500 nm

Preferred Spot Size: 9.5 – 17.25 mm

Aperture: Removed

Iris Adapter: Installed

A centering iris is used to position the vial or
sample cell on the sample window.

A precise, repeatable X-Y mechanism is used to move the sample trays into position for analysis. An
overview of sampling methods is provided, for users who are familiar with Metrohm NIRSystems XDS
instruments. This chart describes the sampling modes, and key selections for each:

Connect to Instrument

Full connection instructions
are provided in section 6.1.

Create DCM

See section 7.1 for
Tablet Transmission.

See section 8.1 for
Reflectance.

Choose the detector
type first. This will set
wavelength range and spot
size to default values.

This DCM shows
“Transmission.”

The default spot size is
9.5mm. This provides
maximum illumination
energy to the tablet.

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