Gas concentrations – single-point calibration – LumaSense Technologies 3434i SF6 Leak Detector User Manual

Page 162

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Chapter 12

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BE6028-14

3434i SF6 Leak Detector

LumaSense Technologies A/S

Page 162 of 191

Fig.12.14b Graph showing a non- linear measurement curve

The question about whether to perform a single- or a two-point span

calibration is difficult to answer, as it is dependent on how linear the

relationship is between a gas’s concentration and the signal it

produces in the cell (see

Fig.12.13

,

Fig.12.14a

and

Fig.12.14b

).

However, we can give you some guidelines on whether you have to

perform a single- or a two-point span-calibration.

·

Single-point calibration should be used when you wish to measure

in the linear range. We define the linear range as the dynamic

concentration range in which you can measure with an error of

5% of the real concentration (this is illustrated in

Fig.12.14b

). For

the most common gases, the linear range is from its detection

limit and up to 10 000 times its detection limit.

·

Two-point calibration is recommended to be used when you wish

to measure in the non-linear range and when you wish to

measure over a dynamic range of 100 000.

Gas Concentrations – Single-point Calibration

If a single-point span-calibration is performed then the span gas

should have a concentration which is at least 100 times its detection

limit and preferable not more than the highest concentration you

expect to measure.

For certain gases it can be inexpedient to use a concentration of at

least 100 times its detection limit, e.g. if you wish to measure a

poisonous gas with a high detection limit, it would be natural to use

a lower concentration. However, this means that the noise and

vibration will have a larger influence on the calibration. This must,

therefore, be taken into account when considering using a lower

concentration.

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