Heidolph LABOROTA 4000 up to 4003 User Manual

Page 74

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Table of contents

72

Laborota 4000 / 4001 efficient, 4010 / 4011 digital, 4002 / 4003 control

1.02

4.5.4 Mounting

the

vertical condenser (G3–G6) to the condenser holder ...................... 92

4.5.5 Installing

the

evaporating flask............................................................................... 93

4.5.6 Adjusting the angle of the evaporating flask .......................................................... 93

4.5.7 Adjusting the immersion depth of the evaporating flask ........................................ 94

4.5.8 Releasing the evaporating flask from the vapour tube........................................... 95

4.5.9 Installing

the inlet pipe............................................................................................ 96

4.5.10 Installing the inlet hose........................................................................................... 96

4.5.11 Installing the receiving flask ................................................................................... 97

4.5.12 Connecting cooling water (not G5)......................................................................... 97

4.5.13 Connecting the vacuum.......................................................................................... 97

4.6 Adding

distillation material ................................................................................................ 102

4.7 Manual

aeration................................................................................................................. 102

4.7.1 Installing/connecting accessories......................................................................... 102

5

Using the Laborota 4000 / 4001 efficient; 4010 / 4011 digital.................................................. 106

5.1

Setting the rotating speed ................................................................................................. 106

5.2

Setting the heating bath temperature................................................................................ 107

5.3

Determining boiling temperature (Laborota 4010 / 4011, optional) .................................. 108

6

Using the Laborota 4002 / 4003 control .................................................................................... 109

6.1

Setting the rotating speed ................................................................................................. 109

6.2

Setting the heating bath temperature................................................................................ 110

6.3

Determining the boiling temperature (with optional boiling temperature sensor) ............. 111

6.4 Controlling

the vacuum ..................................................................................................... 111

6.4.2 p

const mode........................................................................................................ 112

6.4.3 T

auto mode ......................................................................................................... 113

6.4.4 p

auto mode ......................................................................................................... 114

6.4.5 Interrupting evacuation......................................................................................... 115

6.4.6 Applying the current value as the setpoint (p const mode only) ......................... 115

6.5 Time

functions ................................................................................................................... 115

6.5.1 Duration................................................................................................................ 115

6.5.2 Timer .................................................................................................................... 116

6.6 Managing

distillation parameters ...................................................................................... 116

6.6.1 Storing

data records............................................................................................. 117

6.6.2 Recalling

data records.......................................................................................... 117

6.7 Ramp

function ................................................................................................................... 117

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