Metrohm 732 IC Detector User Manual

Page 146

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5.2 Maintenance and servicing

732 IC Detector / 733 IC Separation Center

139

4 Rinse with dist. H

2

O

•

Rinse IC system with dist. Or demin. Water (flow rate

1 mL/min) for ca. 10 min.

5 Rinse with eluent

•

Rinse IC system with the eluent needed for the separating

column you intend to install until the absolute conductivity

displayed on the 732 IC Detector is stable.

6 Remove coupling

•

Remove 6.2620.060 Coupling between column outlet capil-

lary 67

67 and inlet capillary 82

82 (see Fig. 16).

7 Connect new column to injector

•

Remove end caps from column 76

76.

•

Screw inlet end of separating column 76

76 (note flow direction)

to column connection capillary 67

67 or to the precolumn (see

section 2.8.4/section 2.8.6).

8 Rinse column

•

Place beaker beneath the column outlet.

•

Switch on 709 IC Pump and rinse column with eluent for ca.

10 min, then switch off pump.

9 Connect column to detector block

•

Screw outlet end of separating column 76

76 to inlet capillary 82

82

or suppressor inlet capillary 89

89.

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