Metrohm 820 IC Separation Center - Manual (Page 122)

6 Appendix
819 IC Detector / 820 IC Separation Center
114
Practical notes ..................................67
Pulsations........................................56, 77
Pump.............................see 818 IC Pump
Pump tubing (6.1826.050)
General information ..........................37
Q
QA .......................................................106
Quality assurance ...............................106
R
Range ............................49, 51, 52, 53, 57
Ready signal .........................................82
Rear
819 ...................................................... 5
820 ...................................................... 7
Rear panel 21
Close rear panel .........................15, 16
Figure .................................................. 8
Replacing rear panel ........................18
Rear panel 28
Figure .................................................. 8
Open rear panel................................32
Rectification of malfunctions ................77
Recycling ........................................68, 70
Reference conditions......................89, 91
Reference temperature.........................87
Regeneration...................................67, 72
Regeneration solution.........37, 45, 46, 72
Remote ..................................................57
Remote configuration ............................58
Remote input lines
Functions ..........................................81
Remote interface 10
Description........................................83
Figure .................................................. 5
Pin assignment .................................83
Remote interface 8
Description........................................81
Pin assignment .................................81
Remote lines ....................................51, 56
Remote output lines
Functions ..........................................82
Replacing the suppressor ....................75
Resolution .......................................66, 77
Rinse with dist. H
2
O ..............................71
Rinse with eluent...................................71
Rinsing of IC system.............................70
Rinsing solution ....................................37
RS 232 interface 22
Figure .................................................. 8
RS 232 interface 9
Baud rate ..........................................79
Data transmission protocol ..............79
Description........................................79
Figure .................................................. 5
Pin assignement ...............................80
S
Safety notes ..........................................12
Safety specifications.......................89, 90
Sample loop 61
Figure ..........................................40, 43
Fill......................................................62
Ordering designation......................103
Selection ...........................................37
Scope of delivery ..................................92
Screw nut 71
Figure................................................ 74
Selection of the sample loop................ 37
Selectivity .............................................. 66
Separating column
Changing .......................................... 71
Characteristic data ........................... 66
Dead volume .................................... 67
Fixing........................................... 40, 44
General information.......................... 34
Install in column heating................... 35
Installation......................................... 40
Mounting........................................... 42
Practical notes .................................. 66
Protection.......................................... 66
Regeneration .................................... 67
Rinsing ........................................ 40, 43
Separation efficiency ........................ 66
Storage ............................................. 67
Separating column 53
Changing .......................................... 71
Figure.................................... 35, 40, 43
Mounting..................................... 40, 43
Separation Center connection 10
Figure.................................................. 5
Serial number 34
Figure.................................................. 8
Serial number 40
Figure.................................................. 9
Serial number 7
Figure.................................................. 5
Service .................................................. 70
Servicing ............................................... 69
Set point ................................................ 64
<Set> .................................................... 65
<SET> .................................................. 56
Setting up the instrument ..................... 13
Shutdown.............................................. 70
Silicone tubing
6.1816.000 .....................94, 96, 97, 99,
100, 101
Single-channel system ..................... 3, 40
Software installation.............................. 27
SOP..................................................... 106
Spilled chemicals ................................. 69
Splitting ........................................... 67, 77
Stability.................................................. 90
Standard chromatogram...................... 66
Standard operating procedures......... 106
Start with startup hardware
Thermostat........................................ 65
Static charges....................................... 12
Step ....................................................... 64
Stirring of the eluent.............................. 68
Sunlight ................................................. 13
Suppression.......................................... 37
Suppressor ...................................... 58, 61
Suppressor holder 75
Figure................................................ 74
Suppressor inlet capillary 64
Figure.......................................... 43, 44
Mounting........................................... 44
Suppressor inlet capillary 65
Figure.......................................... 43, 44
Mounting........................................... 45
Suppressor inlet capillary 68
Figure.......................................... 43, 44
Mounting........................................... 46
Suppressor module 70
Cleaning............................................ 73
Connection 1 .................................... 45
Connection 2 .................................... 45
Connection 3 .................................... 46
Connection of column...................... 42
Connections ..................................... 44
Figure................................................ 43
General information.......................... 37
Mounting........................................... 44
Protection ......................................... 69
Regeneration .................................... 72
Replacement .................................... 75
Suppressor outlet capillary 66
Figure.......................................... 43, 44
Mounting..................................... 45, 46
Suppressor outlet capillary 67
Figure.......................................... 43, 44
Suppressor outlet capillary 69
Figure.......................................... 43, 44
Mounting........................................... 45
Suppressor rotor 74
Figure................................................ 74
Ordering designation ..................... 103
Syringe
Connection ......................................... 6
Syringe (6.2816.020)
Connection of syringe ...................... 19
Ordering designation .......... 95, 97, 98,
100, 101, 102
T
Technical data ...................................... 87
Temperature
of column heating ............................ 64
of thermostat .................................... 64
Temperature coeff. ................................ 55
Temperature coefficient ....................... 87
Temperature control
Column heating................................ 90
Temperature correction........................ 87
Temperature dependence ................... 87
Temperature deviation ......................... 88
Temperature range............................... 90
Temperature stability...................... 55, 88
Terminal block 26
Pin assignment................................. 86
Terminal block 31
Pin assignment................................. 86
Test chromatogram.............................. 34
Thermostat ................................ 51, 55, 64
actual temperature ........................... 64
operating temperature ..................... 64
Thermostat lamp 12
Figure.................................................. 6
Thermostatting ..................................... 88
Transport .............................................. 13
Transport damage.............................. 107
Treatment of eluents ............................ 68
Triggering of functions ......................... 81
Tubing connections
Connection to injection valve........... 31
Two-channel system .................. 3, 41, 47
V
Validation ............................................ 106
Valve A.................................................. 61
Terminal block 31............................... 8
Valve B.................................................. 61
Terminal block 26............................... 8
Valve interfaces .................................... 86