Operation, Interfaces, Appendix – Metrohm 820 IC Separation Center User Manual

Page 6

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Table of contents

819 IC Detector / 820 IC Separation Center

II

3

Operation ......................................................50

3.1

819 IC Detector ....................................................................... 50

3.1.1

819 IC Detector icon ................................................................... 50

3.1.2

Settings in the "819 IC Detector" window.................................... 50

3.2

820 IC Separation Center ....................................................... 60

3.2.1

820 IC Separation Center icon.................................................... 60

3.2.2

"820 IC Separation Center" window ............................................ 60

4

Notes – Maintenance – Faults ......................66

4.1

Practical notes on ion chromatography ................................ 66

4.1.1

Separating columns .................................................................... 66

4.1.2

Pumps ......................................................................................... 67

4.1.3

Eluents......................................................................................... 68

4.1.4

Suppressor module..................................................................... 69

4.1.5

Connections ................................................................................ 69

4.2

Maintenance and servicing .................................................... 69

4.2.1

General information..................................................................... 69

4.2.2

Passivation .................................................................................. 70

4.2.3

Recycling..................................................................................... 70

4.2.4

Shutdown .................................................................................... 70

4.2.5

Changing separating columns ................................................... 71

4.2.6

Regeneration of suppressor ....................................................... 72

4.2.7

Cleaning the suppressor............................................................. 73

4.2.8

Replacement of suppressor module .......................................... 75

4.3

Faults and malfunctions ......................................................... 77

4.3.1

Malfunctions and their rectification ............................................. 77

5

Interfaces .....................................................79

5.1

RS 232 interface...................................................................... 79

5.1.1

Data transmission protocol......................................................... 79

5.1.2

Pin assignment............................................................................ 80

5.2

Remote interfaces................................................................... 81

5.2.1

"Remote" interface....................................................................... 81

5.2.2

"IC Separation Center" interface.................................................. 83

5.3

Analog output.......................................................................... 85

5.4

External power supply for 820 IC Separation Center .......... 85

5.5

Valve interfaces....................................................................... 86

6

Appendix .......................................................87

6.1

Technical data......................................................................... 87

6.1.1

819 IC Detector ........................................................................... 87

6.1.2

820 IC Separation Center............................................................ 90

6.2

Scope of delivery .................................................................... 92

6.2.1

819 IC Detector ........................................................................... 92

6.2.2

820 IC Separation Center............................................................ 94

6.3

Optional accessories ............................................................ 103

6.3.1

Accessories for 820 IC Separation Center ............................... 103

6.3.2

Column heating......................................................................... 104

6.3.3

Cable ......................................................................................... 105

6.3.4

Literature.................................................................................... 105

6.4

Validation / GLP .................................................................... 106

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