5 • service – Oritron Dionex Ion Chromatography System ICS-2100 User Manual

Page 6

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ICS-2100 Ion Chromatography System

iv

Doc. 065291-01 3/09

4.10 Nonreproducible Peak Height or Retention Time . . . . . . . . . . . . . . . . .94

4.11 Abnormal Retention Time or Selectivity . . . . . . . . . . . . . . . . . . . . . . . .94

4.12 No Cell Response . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .94

4.13 High Cell Output . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .95

4.14 Baseline Noise or Drift . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .96

4.15 Vacuum Degas Assembly Does Not Run . . . . . . . . . . . . . . . . . . . . . . . .97

5 • Service

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .99

5.1

Diagnostic and Calibration Procedures . . . . . . . . . . . . . . . . . . . . . . . . .99

5.1.1

Chromeleon Wellness Panel Overview . . . . . . . . . . . . . . . . . .100

5.1.2

Diagnostic and Calibration Touch Screen Overview . . . . . . .102

5.1.3

Calibrating the Conductivity Cell . . . . . . . . . . . . . . . . . . . . . .103

5.1.4

Calibrating the Flow Rate . . . . . . . . . . . . . . . . . . . . . . . . . . . .106

5.1.5

Calibrating the Vacuum Degas Assembly . . . . . . . . . . . . . . . .108

5.2

Isolating a Restriction in the Liquid Lines . . . . . . . . . . . . . . . . . . . . . .109

5.3

Replacing Tubing and Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .113

5.4

Rebuilding the Injection Valve or Auxiliary Valve . . . . . . . . . . . . . . .114

5.5

Replacing an Auxiliary Valve Pod . . . . . . . . . . . . . . . . . . . . . . . . . . . .116

5.6

Cleaning and Replacing the Pump Check Valves . . . . . . . . . . . . . . . .118

5.7

Replacing a Pump Piston Seal and Piston Rinse Seal . . . . . . . . . . . . .120

5.8

Replacing a Pump Piston . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124

5.9

Replacing the Waste Valve or Priming Valve O-Ring . . . . . . . . . . . . .125

5.10 Replacing the Conductivity Cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .127

5.11 Replacing the Suppressor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .130

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