Metrohm 756 KF Coulometer User Manual

Page 36

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3.6 Parameters, key <PARAM>

756/831 KF Coulometer, Instructions for Use

28

stop crit: rel.drift

**titr.




stop drift 5 ug/min

**titr.

rel.drift 5 ug/min

**titr.

Type of stop criteria (drift, rel.drift)

Drift: the entered value corresponds to the stop drift.

rel.drift: the stop drift is calculated according to the

"actual drift at start of titration + entered value, see

page 32.

If

Drift

has been set:

Switches off titration when EP and stop drift have been

reached (1...999 ug/min)

If

rel.drift

has been set:

Switches off titration when EP and corresponding drift

have been reached (0...999 ug/min)


>titration parameters

pause 0 s

**titr.



extr.time 0 s

**titr.





start drift 20 ug/min



I(pol): 10 uA




electrode test: ON




temperature 25.0 °C

cond.


time interval 2 s

cond.



max.titr.time OFF s

**titr.

Titration parameters

Pause (0...999 999 s)

Waiting period in which no iodine is produced. The

pause can be terminated with <QUIT>.

Extraction time (0...999 999 s)

The titration takes place during this time. However, it is

not stopped until the extraction time has elapsed (even

when the EP has been reached). The extraction time

can be terminated with <QUIT>.

Start Drift (1...999 ug/min)

Drift value below which the start of the titration is pos-

sible (conditioning OK), see page 32.

Polarization current (2, 5, 10, 20, 30 uA),

at the indicator electrode. The set standard value

should be optimal for most applications, see also page

32.

Electrode test (OFF, ON)

Performed on changeover from the inactive standby

state to a measurement.

OFF

means that the test is not

performed.

Titration temperature (-170.0...500.0 °C)

for the documentation of titration conditions.

Time interval (1...999 999 s)

Time interval for acquisition of a measured value into

the measuring point list.

Maximum titration time (1...999 999 s, OFF)

Safety time for termination of the titration even when

the EP has not been reached.

The titration time corresponds to the time in which con-

trol is carried out, i.e. inquiries after the start without

control and pause periods are not included in this

time.

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