All plateaus negative – Agilent Technologies Quaternary Pump 1100 Series User Manual

Page 94

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94

Troubleshooting and Test Functions

Evaluating the Results

All plateaus negative

First plateau positive, second and third plateau negative

Potential Cause

Corrective Action

Loose or leaky fittings.

Ensure all fittings are tight, or exchange
capillary.

Loose purge valve.

Tighten the purge valve (14mm wrench).

Contaminated purge valve.

Open and close purge valve to flush out
contamination. Exchange the valve if still
leaky.

Loose pump head screws.

Ensure the pump head screws are tight.

Leaking seals or scratched plungers.

Exchange the pump seals. Check the plungers
for scratches. Exchange if scratched.

Leaking outlet valve.

Exchange the outlet valve.

Leaky damper.

Exchange damper.

Potential Cause

Corrective Action

Air in pump or new seals not yet seated.

Flush pump thoroughly with isopropanol under
pressure (use restriction capillary).

Loose active inlet valve.

Tighten the active inlet valve (14mm wrench).
Do not overtighten!

Loose pump head screws.

Ensure the pump head screws are tight.

Loose outlet valve.

Ensure the sieve in the outlet valve is installed
correctly. Tighten the outlet valve.

Leaking seal or scratched plunger.

Exchange the pump seals. Check the plungers
for scratches. Exchange if scratched.

Defective active inlet valve.

Exchange the active inlet valve.

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