Metrohm 781 pH/Ion Meter User Manual

Page 126

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8.2 Messages

116

780/781 pH/Ion Meter, Manual

Message

Situation

Cause

Remedy

XXX bytes
missing

Method storing

XXX bytes are missing for
saving a method

Press

<QUIT>

to delete

old methods

V add too
large

Conc calibration,
standard addition

Standard volume to be
added is larger than buret
volume

Use larger buret

Reduce start volume

Increase standard con-

centration

V add too
small

Conc calibration,
standard addition

Standard volume to be
added is too small

Check parameters (see

Section 6.5.5 or 6.6.1)

Reduce standard con-

centration

Use smaller buret

check working
cond.

Standard addi-
tion,
sample addition

No change in potential
after standard addition

Check standard addition

Strongly drifting electrode
signal

Check electrode

Slope sign incorrect for
type of ion

Check ion parameters under

Section 6.5.2

evaluation er-
ror

Conc calibration,
standard addition,
sample addition

Evaluation not possible

Check parameters

Check standards

please wait

Report output

New task was started dur-
ing report output

Wait for report output

delta T >2 °C pH calibration,

Conc calibration

Temperature difference
between two buffers or
standards is too large

1. Match temperatures
2. Continue with

<ENTER>

or cancel

with

<MODE>

and re-

start

Electrode test

Temperature difference
between two buffers is too
large

1. Cancel electrode test with

<MODE>

2. Restart with suitable buff-

ers

check elec-
trode

Temperature
measuring

Short circuit or interruption Remedy fault or change

mode

electrode test
not passed

Electrode test

Electrode test gives values
outside the tolerances

see

Section 8.6.4

validate in-
strument

Instrument has
been switched on

Set validation interval has
expired

1. Validate instrument
2. Reset time counter to ze-

ro (see

Section 5.5

)

same buffer

pH calibration

Potential difference be-
tween 1st and 2nd buffer is
too small

1. Change buffer
2. Press

<ENTER>

same standard Conc calibration

Pot. difference between 1st
and 2nd standard < 6 mV

1. Change standard
2. Press

<ENTER>

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