1 method "pc" and "pc seg – Metrohm 788 IC Filtration Sample Processor User Manual

Page 107

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4.6 Standard methods

788 IC Filtration Sample Processor

99

4.6.1 Method "PC" and "PC Seg"

Application

Processing a queue with the PC program with the PC as "Master".

Interconnection

See section 2.6.1 (without suppression) and section 2.6.3 (with sup-

pression)

Program of 788 IC Filtration Sample Processor

788 IC Filtr. Proc. 5.788.0010
parameters
method PC
number of samples: rack
>start sequence
1 CTL:Rm: INIT
>sample sequence
1 SCN:Rm : Wait1
2 SCN:Rm : Pump1 ?
3 MOVE 1 : sample
( PUMP 1.1 : 5 s)
4 LIFT: 1 : work mm
5 CTL:Rm: FILL A 1
6 PUMP 1.1 : 240 s
7 CTL:Rm: ZERO 1
8 CTL:Rm: INJECT A 1
>final sequence
>changer settings
rack number 0
lift rate 1 12 mm/s
shift rate 20
>manual stop
CTL Rmt: **************
CTL RS232:
------------

 Report header with serial number and program ver-

sion

 Method name
 Number of samples to be processed (entire sample

rack)

 Initialize remote interface


 Waiting until 732 IC Det. sends signal on rem. line 3
 Waiting until 709 IC Pump runs
 Move needle to sample
 Only "PC Seg": aspirate air during 5 s
 Place lift with needle to working position
 Switch injection valve A at 733 to "Fill"
 Fill sample loop with sample during 240 s
 Trigger autozero at 732 IC Detector
 Switch injection valve A at 733 to "Inject"

 —— Settings for changer functions ——




 —— Reaction to manual stop ———


Settings in the «IC Metrodata» program

Definition of IC method (analysis time, start parameters for IC instru-

ments 732, 733 and 709, etc.), additional association of this method

with the following time program for the 732 IC Detector:

Method / Equipment / Setup / Program / Text:

0.0 Puls_788_set Set remote line 3 at 732/1 to 1 (s. below)
0.1 Puls_788_reset Set remote line 3 at 732/1 to 0 (s. below)
0.2 Flag

end

Program end

Method / Equipment / Setup / Program / Remote configuration:

Puls_788_set =

**1***** Set remote line 3 at 732/1 to 1

Puls_788_reset =

**0***** Set remote line 3 at 732/1 to 0

Method / Equipment:

Start with method

Procedure at program start

1. Start 788 IC Filtration Sample Processor with <START>.
2. Create new queue in the program «IC Metrodata» and start it.

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