Metrohm 788 IC Filtration Sample Processor - Manual (Page 113)

4.6 Standard methods
788 IC Filtration Sample Processor
105
Program of 788 IC Filtration Sample Processor
788 IC Filtr. Proc. 5.788.0010
parameters
method Preconc
number of samples: rack
>start sequence
1 CTL:Rm: INIT
2 CTL:Rm: INJECT A 1
3 CTL:Rm: PUMP 752 ON
>sample sequence
1 SCN:Rm : Wait1
2 SCN:Rm : Pump1 ?
3 MOVE 1 : sample
4 LIFT: 1 : work mm
5 PUMP 1.1 : ON s
6 WAIT 60 s
7 CTL:Rm: FILL A 1
8 WAIT 120 s
9 PUMP 1.1 : OFF s
10 CTL:Rm: ZERO 1
11 CTL:Rm: INJECT A 1
>final sequence
1 WAIT 1200 s
2 CTL:Rm: PUMP 752 OFF
>changer settings
rack number 0
lift rate 1 12 mm/s
shift rate 20
>manual stop
CTL Rmt: **************
CTL RS232:
------------  Report header with serial number and program ver-
sion
 Method name
 Number of samples to be processed (entire sample
rack)
 Initialize remote interface
 Switch injection valve A at 733 to "Inject"
 Switch 752 Pump Unit on for suppression
 Waiting until 732 IC Det. sends signal on rem. line 3
 Waiting until 709 IC Pump runs
 Move needle to sample position
 Place lift with needle to working position
 Switch on pump at 788
 Waiting time 60 s
 Switch injection valve A at 733 to "Fill"
 Sample preconcentration during 120 s (preconcen-
tration time must be adapted)
 Switch off pump at 788
 Trigger autozero at 732 IC Detector
 Switch injection valve A at 733 to "Inject"
 Wait for final regeneration of suppressor
 Switch 752 Pump Unit off
 —— Settings for changer functions ——
 —— Reaction to manual stop ———
Settings in the «IC Metrodata» program
Definition of IC method (analysis time, start parameters for IC instru-
ments 732, 733 and 709, etc.), additional association of this method
with the following time program for the 732 IC Detector:
Method / Equipment / Setup / Program / Text:
0.0 Puls_788_set Set remote line 3 at 732/1 to 1 (s. below)
0.1 Puls_788_reset Set remote line 3 at 732/1 to 0 (s. below)
0.2 Flag
end Program end
Method / Equipment / Setup / Program / Remote configuration:
Puls_788_set = **1***** Set remote line 3 at 732/1 to 1
Puls_788_reset = **0***** Set remote line 3 at 732/1 to 0
Method / Equipment:
Start with method
Procedure at program start
1. Start 788 IC Filtration Sample Processor with <START>.
2. Create new queue in the program «IC Metrodata» and start it.