Metrohm 788 IC Filtration Sample Processor User Manual

Page 148

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6 Appendix

788 IC Filtration Sample Processor

140

Do not connect the dialysis cell with anything other than the

6.2744.000 PVDF compression fittings supplied. If 6.2744.010

PEEK compression fittings are used, stress cracks may appear in the

ultra-filtration cell !

4 Close ultra-filtration cell

x Insert sealing ring in the appropriate recess in top part 43

43

43

43.

x Place top part on bottom part 45

45

45

45 so that both parts lie flush.

x Using the 6.2621.070 Allen key, screw the 5 screws 46

46

46

46 right

in and tighten up.

5 Attach ultra-filtration cell

x Insert the assembled ultra-filtration cell in the cell holder 26

26

26

26

according to Fig. 1 or Fig. 11. The heads of the five screws

46

46

46

46 fit to the small holes of the cell holder.

x Connect all three tubings according to step 3 to 5 in section

2.3.9 to the corresponding inlet and outlet openings of the ul-

tra-filtration cell by using PVDF compression fittings 22

22

22

22.

6 Rinse ultra-filtration cell

x Every time the filtration membrane is changed, the remaining

air in the cell and tubings has to be removed. This can be

done by rinsing with ultrapure water.

x A completely installed 788 IC Filtration Sample Processor with

ultra-filtration cell is required for processing the following

steps. The rinsing solution (e.g. ultrapure water) is stored in a

300 mL PE bottle on the special beaker position 1. The 788 IC

Filtration Sample Processor is online and in normal state. The

pump is switched of (display: 'PUMP–') and the 788 is ready

for use (display: 'ready').

x Turn the sample rack to position the beaker with the rinsing

solution under the needle by pressing <MOVE> followed by

choosing 'spec.1' with <SELECT>.

x Lower the lift into rinse position with <LIFT> and <SELECT>

'rinse'

x Turn on the pump by pressing <PUMP>. All connected tub-

ings and the ultra-filtration cell will be rinsed.

x After adequate time (e.g. 5 min.), switch off the Pump

(<PUMP>) and raise the lift to its rest position by pressing

<HOME>.


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