Calibration checks with zero/span valves, Perform the zero/span check, Step one – Teledyne 9110TH - Nitrogen Oxides Analyzer User Manual

Page 201: Step two

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Calibration Procedures

Model 9110TH NOx Analyzer

Teledyne Analytical Instruments

181

5.6. CALIBRATION CHECKS WITH ZERO/SPAN VALVES

Zero and span checks using the zero/span valve option are similar to that described in
Section 7.4, except that zero air and span gas are supplied to the analyzer through the
zero gas and span gas inlets from two different sources.

Informal calibration checks, which only evaluate but do not alter the analyzer’s response
curve, are recommended as a regular maintenance item and in order to monitor the
analyzer’s performance. To carry out a calibration check rather than a full calibration,
follow these steps.

To perform a manual calibration check with zero/span valve:

STEP ONE:

Connect the sources of Zero Air and Span Gas as shown in section 7-4.

STEP TWO:

Perform the zero/span check.

The ZERO and/or SPAN

keys will appear at various

points of this process.

It is not necessary to press

them.

Set the Display to show

the NOX STB test

function.

This function calculates

the stability of the NO/NO

x

measurement

Toggle TST> button until ...

Allow zero gas to enter the sample port

at the rear of the analyzer.

Wait until NOX STB
falls below 0.5 ppm.

This may take several

minutes.

Allow span gas to enter the sample port

at the rear of the analyzer.

Wait until NOX STB
falls below 0.5 ppm.

This may take several

minutes.

Record NO

X

, NO, NO

2

or O

2

zero point

readings

Record NO

X

, NO, NO

2

or O

2

span point

readings

SAMPLE

A1:NXCNC1=100PPM

NOX=XXX.X

< TST

TST >

CAL CALZ

CALS

SETUP

SAMPLE

A1:NXCNC1=100PPM

NOX=XXX.X

< TS

T TST > CAL CALZ CALS

SETUP

SAMPLE

A1:NXCNC1=100PPM

NOX=XXX.X

< TS

T TST > CAL

CALZ

CALS

SETUP

SAMPLE

GAS TO CAL:NOX

NOX

O2

ENTR

EXIT

SAMPLE

RANGE TO CAL:LOW

LOW

HIGH

ENTR

EXIT

Analyzers enters

ZERO cal

mode.

SAMPLE

A1:NXCNC1=100PPM

NOX=XXX.X

< TS

T TST > CAL

CALZ

CALS

SETUP

SAMPLE

GAS TO CAL:NOX

NOX

O2

ENTR

EXIT

SAMPLE

RANGE TO CAL:LOW

LOW

HIGH

ENTR

EXIT

Analyzers enters

SPAN cal

mode.

SPAN CAL M

NOX STB= XXX.X PPM

NOX=X.XXX

<TST TST> ZERO SPAN CONC

EXIT

SAMPLE

A1:NXCNC1=100PPM

NOX=XXX.X

< TS

T TST > CAL CALZ CALS

SETUP

ZERO CAL M

NOX STB= XXX.X PPM

NOX=XXX.X

<TST TST>

ZERO

CONC

EXIT

ZERO CAL M

NOX STB= XXX.X PPM

NOX=XXX.X

<TST TST>

ZERO

CONC

EXIT

Return to
SAMPLE

Display

SPAN CAL M

NOX STB= XXX.X PPM

NOX=XXX.X

<TST TST>

ZERO

CONC

EXIT

Return to
SAMPLE

Display

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