Performing routine measuring work, H_1928, H_2449 – BUCHI DuMaster D-480 User Manual

Page 140: O_3676, Ge 140), Age 140)

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Operation Manual D-480

©BÜCH Labortechnik AG

7 - Using the instrument

140

 Save the data or print them out. See Data backup and printing (on page 158).

When can routine measuring work be omitted?

You can measure real samples without preceding routine measuring work:

if you have already performed routine measuring work today

if measuring breaks last less than 2 hours.

Measuring real samples without preceding routine measuring work

Please observe the following instruction:

Caution

Inserting multiple samples into the ball valve (only for

solid operation)

If there are samples in the carousel while you are changing the position of the
carousel via System > Sample Position, multiple samples may fall into the ball
valve at the same time. In this case, a service technician is required.

Before changing the position of the carousel, always remove all samples from the
carousel.

Proceed as follows:

 Move the empty carousel to zero position. To do so, open the "Set carousel position" dialog in

the operating software by selecting System > Sample Position.

 Select the radio button next to "Reference run" and click OK. The carousel moves to zero

position.

 Prepare the samples. Cf. Sample preparation instructions (on page 126).

 Insert the samples on the carousel.

 Enter the weight in [mg] in the sample view (text view) on the PC if it has not already been

transmitted online by the balance.

 Enter the sample name (max. 32 characters) in the sample view (text view).

 Select a suitable method. See Values for oxygen dosing (on page 137).

 Go through the measuring start checklist. See Checklist for real sample measurement (on

page 142).

 Start the analysis process in the operating software:

Select System > Auto run to start a multiple-sample analysis.

Select System > Single run to start a single-sample analysis.

 Once measurement is finished, evaluate the measurement.

 Save the data or print them out. See Data backup and printing (on page 158).

Performing routine measuring work

Overview

This section provides information about

types of routine measuring work,

the purpose of routine measuring work,

and how to perform this routine measuring work depending on the mode.

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