Analytical characteristics, Technical specifications, O_3614 – BUCHI DuMaster D-480 User Manual

Page 31: O_3615

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Operation Manual D-480

©BÜCH Labortechnik AG

3 - Product description

31

Analytical characteristics

Analytical characteristics

The following table explains the analytical characteristics:

Analytical characteristic

Comments

Analysis method

Nitrogen determination from a sample according to Dumas.
Combustion of the samples, transfer to N

2

, separation of foreign

gases, thermal conductivity detection.

Standards

Analysis method according to:
AOAC 99.03, AOAC 993.13, AOAC 968.06, AOAC 992.15,
AOAC 992.23, ASBC, AACC (for fertilizer, meat, meat products,
grain, oilseed, brewery grain, flour, animal feed),
DIN 10 467, milk and milk products,
EN 61010, DIN projected.

Detector

Thermal conductivity detector (TCD).

Sample weight/sample volume

Up to 1 g organic substance or approx. 1 ml sample volume
(depending on substance).

Dynamic work range

0.1 mg bis 200 mg N abs.

Precision

Less than 0.5 % relative standard deviation with test substance
aspartic acid (sample weight: approx. 300 mg).

Detection limit

0.10 mg N abs.

Recovery rate

Larger than 99.5 % for test substances.

Duration of analysis

Self-optimizing, 4 to 6 minutes, depending on substance and
sample weight (e.g 5,5 min. for 0.4 g hay).

Calibration

Linear and non-linear curve adjustment; total work range, if
applicable divided into two segments.

Data storage and data output

Storage on hard disk or external storage media.
LIMS transfer possible.
Data output to screen and printer.

Technical specifications

Standardization

The instrument conforms to CE standards in accordance with EC Directives:

EMC 89/336/EEC

LVD 73/23/EEC

Control and data processing

The following table contains the technical specifications of the control and data processing system:

Reference value

Technical specifications

Control and evaluation unit

PC with operating system Windows XP Professional or a newer
version of Windows Professional
Printer (optional)

Software

German or English
Menu-driven
Status display during analysis
Real-time graphics

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