Min 2, Fv t, No f x ] [no = f – Teledyne 9110T - Nitrogen Oxides Analyzer User Manual

Page 226

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Model 9110T NOx Analyzer

EPA Protocol Calibration

Teledyne Analytical Instruments

226

2. Determine the volume (cm3) of the calibrator reaction cell (VRC). If the actual

volume is not known, estimate the volume by measuring the approximate
dimensions of the chamber and using an appropriate formula.

3. Determine the required minimum total flow output (FT) :

Equation

10-2

F

T

= analyzer flow demand (cm

3

/min) x 110/100

 If more than one analyzer is to be calibrated at the same time, multiply FT by

the number of analyzers.

4. Calculate the NO concentration [NO]

OUT

needed to approximate 90% of the URL of

the NO

2

analyzer to be calibrated:

Equation

10-3

[NO]

OUT

= URL of analyzer (ppm) x 90/100

5. Calculate the NO flow (F

NO

) required to generate the NO concentration [NO]

OUT

:

Equation 10-4

]

[NO

F

x

]

[NO

=

F

STD

T

OUT

NO

6. Calculate the required flow through the ozone generator (F

O

):

Equation 10-5

F

-

-

ppm

2.75

V

X

F

X

]

[NO

=

F

NO

RC

NO

STD

o

min

7. Verify that the residence time (t

R

) in the reaction cell is <2 min:

Equation 10-6

min

2

NO

O

RC

R

F

F

V

t

8. Verify that the dynamic parameter specification (P

R

) of the calibrator's reaction cell

is >2.75 ppm-min:

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