Oritron Dionex Ion Chromatography System ICS-2100 User Manual

Page 101

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4 • Troubleshooting

Doc. 065291-01 3/09

89

4. Check the Degas settings. Select either the Monitor option or the

Cycle option. If you select Cycle, set the time On to 30 seconds and
the time Off to 600 seconds. If Cycle is already selected, try
increasing the time on or decreasing the time off.

NOTE Degas options can also be selected from the

touch screen

PUMP

page (see

Section B.7

).

End-line filter is dirty or clogged

When new, end-line filters (P/N 045987) are pure white. If the system is in
continuous operation, change the end-line filter weekly, or whenever it
becomes discolored. Replace the filter more often if bacterial buildup is
visible or if the eluent does not contain solvent.

NOTE It is especially important to regularly replace end-line

filters when using aqueous eluents, which may
contaminate the filter with bacteria or algae. The
bacterial buildup may not be visible.

Blockages in inlet tubing

Kinked or clogged tubing causes the pump to be “starved” for eluent. Replace
the tubing and fittings (see

Section 5.3

).

Dirty check valve

Clean or replace the pump check valve (see

Section 5.6

).

Liquid leaks at junction between pump head and pump casting

Use the open-end wrench (P/N 014605) provided in the ICS-2100 Ship Kit
(P/N 064375) to tighten the two acorn nuts that attach the pump head to the
pump housing (see

Figure 5-13

). Tighten the nuts evenly (12 in-lb torque).

If the leak persists, replace the piston seal (see

Section 5.7

).

Liquid leaks from the seal wash port

Replace the piston seal (see

Section 5.7

).

Scratched pump piston

Check the pump pistons for scratches and replace if necessary (see

Section 5.8

).

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