8 excessive system backpressure, Excessive system backpressure – Oritron Dionex Ion Chromatography System ICS-2100 User Manual

Page 104

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ICS-2100 Ion Chromatography System

92

Doc. 065291-01 3/09

Damaged piston seal

Replace the piston seal (see

Section 5.7

).

Dirty pump check valve

Clean or replace the check valve (see

Section 5.6

).

Leaking liquid lines or fittings

Check the liquid lines and fittings for small leaks. Tighten or, if necessary,
replace the liquid line connection (see

Section 5.3

). Refer to Installation of

Dionex Liquid Line Fittings (Document No. 031432) for tightening
requirements. The manual is included on the Dionex Reference Library CD-
ROM (P/N 053891).

4.8

Excessive System Backpressure

Restriction in the system plumbing

Check all liquid lines for crimping or blockage. Make sure the ferrule fittings
are not overtightened onto tubing. Refer to Installation of Dionex Liquid Line
Fittings
(Document No. 031432) for details. The manual is included on the
Dionex Reference Library CD-ROM (P/N 053891).

If you have trouble isolating the restriction, refer to

Section 5.2

.

Plugged or damaged fitting

Isolate the faulty fitting by loosening fittings, one by one, until the pressure
returns to normal. Repair or replace the fitting (see

Section 5.3

).

Flow rate through the columns too high

Set the correct rate for your application. If an incorrect flow rate calibration is
suspected, calibrate the flow (see

Section 5.1.4

).

Clogged column bed supports

Refer to the instructions in the column manual for troubleshooting guidance.
Column manuals are included on the Dionex Reference Library CD-ROM
(P/N 053891).

Contaminated columns

Clean the columns as instructed in the column manual or replace the guard
column.

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