246 meas, O, s, M, a – Metrohm 746 VA Trace Analyzer User Manual

Page 397

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5.7 Program instructions

746 VA Trace Analyzer / 747 VA Stand

5-246

MEAS

Page:

O, S

Stand:

M, A

Abbreviation:

M

Instructions t/s Main parameters Auxiliary parameters

––––––––––––– ––––– ––––––––––––––––––––––––– –––––––––––––––––––––––––

## .. MEAS ..... U.meas ........mV

Function

Application of a constant voltage to the electrodes and measurement of
the current without measured value storage.

Application

The

MEAS

instruction is primarily used together with the HMDE or RDE

for electrochemical enrichment in stripping voltammetry.

Parameter

Range; Default value / Meaning

U.meas

-3000...3000 mV; -

Measurement voltage

The voltage entered here is applied to the electrodes. This voltage
remains in force even after the line time has elapsed until a SWEEP
instruction follows or until it is switched off by

ØMEAS

or

END

in the main

program on the "OP.SEQUENCE" page.

Description

The

MEAS

instruction applies the voltage defined in the

U.meas

para-

meter to the electrode. At the same time, the current measurement is
started in accordance with the parameters defined in the measurement
mode. The duration of the measurement is defined with the line time.

During an ongoing measurement with

MEAS

, the current measured

values for voltage and current are displayed in the measurement window
on the "MONITORING" page (see section 5.5.1).

Comments

The electrode type must be defined before the

MEAS

instruction.

Admissible are

DME

,

SMDE

,

HMDE

or

RDE

.

The measurement mode must be defined before the

MEAS

instruc-

tion. Admissible are

DCTMODE

,

DPMODE

,

AC1MODE

,

AC2MODE

,

SQWMODE

,

CYCMODE

or

PSAMODE

.

If the measured values in measurement of the current should be
plotted, the

TSWEEP

instruction must be used in place of the

MEAS

instruction. However, this must not be in the same segment as the
measurement sweep.

If the measurement voltage

U.meas

should not be switched off at the

end of the program, enter a suitable standby voltage

U.standby

in a

ØMEAS

instruction.

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