Metrohm 746 VA Trace Analyzer User Manual

Page 63

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3 Installation

746 VA Trace Analyzer / 747 VA Stand

3-36

For the addition of a second auxiliary solution we recommend the use of the fol-

lowing accessories:

•

• 1 ×× 6.1446.070 Stopper, with M6 thread
•

• 1 ×× 6.1819.000 PTFE tube, length L = 77 mm, i.d. = 0.8 mm
•

• 2 ×× 6.1805.100 FEP tubing, length L = 40 cm, i.d. = 2 mm
•

• 1 ×× 6.1808.000 Coupling

To install these accessories and ready the 685 Dosimat for automatic dispensing,

proceed as follows:

1 Mount Exchange unit on 685 Dosimat

•

Procedure, see section 2 of 685 Instructions for Use.

2 Insert PTFE tube in 747 VA Stand

•

Remove stopper 25

25 from pipetting opening 75

75 and insert 6.1446.070

stopper (optionally available) into this opening (see Fig. 9).

•

Cut 6.1819.000 PTFE tube (optionally available) to a length of ca. 30 mm

(the tip of the tube should never be immersed into the solution).

•

Insert PTFE tube from above into the 6.1446.070 stopper.

3 Change Exchange unit

•

Screw 6.1805.100 FEP tubing (optionally available) into the threaded

opening of the 6.1446.070 stopper.

•

Screw a 1808.000 Coupling (accessory of 747 VA Stand) to the other end

of the 6.1805.100 FEP tubing and insert this in a slot of the tubing holder

at the rear of the 747 VA Stand.

•

Unscrew the 6.1543.050 Burette tip from the 6.1805.100 FEP tubing

attached to the connection 2 of the Exchange unit (see section 3.9.2).

•

Screw the other end of the 6.1805.100 FEP tubing attached to the Ex-

change unit to the 6.1808.000 Coupling just inserted in the tubing holder

of the 747 VA Stand.

4 Initialize Dosimat(s)

•

Switch on 746 VA Trace Analyzer using the mains switch 11

11.

•

Select dialog page "DOSIMATS".

•

Set parameter

V.init

to

0.00 mL

.

•

Set parameter

V.tube in

to

1.7 mL

.

•

Set parameter

V.tube out

to

3.0 mL

.

•

Press softkey

<Prime all>

for initializing all attached Dosimats or select

desired Dosimat with the cursor keys and press softkey

<Prime Dosimat>

:

The burette cylinder is filled and excess solution is expelled to the meas-

uring vessel. With standard accessories, all tubings to the measuring

vessel will have been filled at the end of the initializing procedure.

•

Start the initializing procedure a second time by pressing the softkey

<Prime all>

or

<Prime Dosimat>

again.

•

Start the initializing procedure a third time by pressing the softkey

<Prime

all>

or

<Prime Dosimat>

again.

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