Metrohm 746 VA Trace Analyzer User Manual

Page 466

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6.2 Preparations before start of a determination

746 VA Trace Analyzer / 747 VA Stand

6-3

•

SEGMENTS

This dialog page is used to define the measured value recording using pro-

gram instructions and their parameters (see section 5.7.3). The most impor-

tant instructions concern selection of the electrode, the measurement mode

and the sweep:

– Electrode

DME

,

SMDE

,

HMDE

,

RDE

– Measurement

DCTMODE

,

DPMODE

,

SQWMODE

,

AC1MODE

,

mode

AC2MODE

,

PSAMODE

,

CYCMODE

– Sweep

SWEEP

,

SSWEEP

,

FSWEEP

,

TSWEEP

,

PSWEEP

,

(CSWEEP...RAMP...CSWEEP)

A total of 8 different segments can be programmed to which the desired sub-

stances can be assigned. The segments are distinguished by their name.

•

SUBSTANCES

On this dialog page maximum 8 different substances with their specific pa-

rameters can be defined. Each desired substance requires the following en-

tries:

– Substance name
– Assignment to a segment

(without assignment, there is no substance evaluation)

– Parameters for substance recognition (Recognition)
– Parameters for baseline calculation (Baseline)
– Definition of the evaluation quantity (Evaluation)
– Parameters for curve display and plot (Display/Plot)
– Parameters for calibration

(standard addition, calibration curve or internal standard)

• CALCULATION

On this dialog page freely selectable calculation formulae for further calcula-

tion of the standard results obtained in the evaluation to produce the desired

final results can be entered.

• DOCUMENTATION

This dialog page is used for definition of the automatic output of reports and

curves on the built-in printer or the printer connected at the parallel or RS232

interface. Further, there is a possibility to enter a detailed comment on the

method.

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